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Pesticide reference standard analysis, sample AD22582, Sept 2001

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Reference standard testing results for pesticide analysis of sample AD22582, verifying analytical method performance with known compounds.

NYC-WTC_000063290–000063355

Folder label: “525 9/24/01 EX 9/29 - 9/30 Analysis”

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Integration Report Quanfile: RUN0929 Quan Entries: 28 Comment: BOHLK; METHOD 525; INST 204; 09/29/01; UNEXTD REF Sorted uia: Entry Number t

No Name of Compound R Time Scantt Mode Peak Areja PR Height 3 chrysene d-12(IS) 22:57 1377 Auto 2,716,948 1,204,097 4 p-terphenyl d-14(IS) 21:02 1262 Auto 3,967,589 1,965,972 5 acenaphthene d-10CSLIRR 12:32 752 Auto 2,706,444 1,766,015 6 phenanthrene d-10(SURR 17:16 1036 Auto 3,876,529 1,959,589 7 chrysene d-12 (SURR) 22:57 1377 Auto 2,716,948 1,204,097 8 1,3-d imethy1-2-n itrobe 8:12 492 Auto 1,571,108 937,500 9 triphenyl phosphate CS 22:19 1339 Auto 1,737,566 693,803 10 perylene d-12 (SURR) 27:31 1651 Auto 1,564,273 290,122 11 hexachlorocyclopentad i 10:23 623 Auto 659,768 464,835 12 hexachlorobenzene 15:43 943 Auto 1,330,658 568,279 13 simazine 16:30 990 Auto 930,775 272,128 14 atrazine 16:41 1001 Auto 836,895 337,234 15 alachlor 18:38 1118 Auto 1,316,995 738,207 16 bis(2-ethyIhexy1)adipa 22:11 1331 Auto 2,295,566 1,016,153 17 b is C2-ethyIhexy1)phtha 23:14 1394 Auto 3,660,981 1,296,439 18 benzo(a Jpyrene 27:15 1635 Auto 2,369,204 471,245 19 eptc 10:47 647 Auto 4,901,212 3,388,884 20 2,6-d in itrotoluene 12:09 729 Auto 958,298 595,786 21 2,4-d ini troto1uene 13:09 789 Auto 1,392,449 697,107 22 mol inate 13:17 797 Auto 2,704,535 1,544,805 23 terbacil 17:39 1059 Auto 493,590 175,642 c o 24 acetochlor 18:27 1107 Auto 899,970 466,379 E 25 metribuzin 18:29 1109 Auto 1,599,775 763,020 o o 26 metolachlor 19:21 1161 Auto 3,848,02b 2,038,432 Q 27 butachlor TO 20:34 1234 Auto 1,152,347 792,592 CM ■c o 28 4,4"-dde 20:57 1257 Auto 1,604,247 1,280,392 CO co Q_ co o o o o 3 o I 0. o O) Id O >- z z

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