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Spiked sample results, sample AD23341, Oct 2001

Machine-extracted title · confidence 90%

Analysis of spiked sample AD23341 to verify recovery rates and analytical accuracy in October 2001.

NYC-WTC_000062659–000062663

Folder label: “525 10/3/01 EX 10/9 - 10/10 Analysis

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Scanned page image, NYC-WTC_000062662
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'2 o o IntesTration Report Quanfile: 23341MSD Quan Entries: 28 ■D c CT o' o O) ro Connent: BOHLK; METHOD 525; INST 204; 10/09/01; SAMPLE 23341 MS "D o O) o> Sorted uia: Entry Nunber t 03 ro O o No Nane of Compound R Tine Scan# Node Peak Area PR Height o c 3 CD 3 chrysene d-12CIS) 22:56 1376 Auto 1,602,631 711,286 3

4 p-terphenyl d-14CIS) 21:01 1261 Auto 3,169,324 2,406,810 5 acenaphthene d-10CSLIRR 12:31 751 Auto 1,385,161 777,439 6 phenanthrene d-10CSLIRR 17:15 1035 Auto 2,401,848 1,096,120 7 chrysene d-12 CSURR) 22:56 1376 Auto 1,602,631 711,286 8 1,3-d inethy1-2-n itrobe 8:11 491 Auto 913,229 522,107 9 triphenyl phosphate CS 22:18 1338 Auto 1,311,011 464,933 10 perylene d-12 CSURR) 27:28 1648 Auto 1,323,337 242,883 11 hexachlorocyclopentad i 10:22 622 Auto 429,937 302,764 12 hexachlorobenzene 15:42 942 Auto 920,723 339,942 13 sinazine 16:29 989 Auto 627,528 186,522 14 atrazine 16:40 1000 Auto 534,235 185,069 15 alachlor 18:37 1117 Auto 886,383 584,057 16 b is C2-ethyIhexy1)ad ipa 22:10 1330 Auto 1,613,288 646,093 17 b is C2-ethyIhexy1)phtha 23:13 1393 Auto 2,772,585 979,729 18 benzo C a)pyrene 27:14 1634 Auto 1,304,214 239,777 19 eptc 10:46 646 Auto 3,499,530 2,377,005 20 2,6-d in itrotoluene 12:09 729 Auto 496,604 230,379 21 2,4-d ini troto1uene 13:08 788 Auto 626,433 318,565 22 no1 inate 13:16 796 Auto 1,568,529 745,620 23 terbac i1 17:39 1059 Auto 775,904 269,916 24 acetochlor 18:26 1106 Auto 642,850 391,346 25 netribuzin 18:28 1108 Auto 718,972 417,553 26 netolachlor 19:21 1161 Auto 2,772,082 1,397,527 27 butachlor 20:33 1233 Auto 877,125 664,843 28 4,4"-dde 20:57 1257 Auto 878,335 481,465

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NYC-WTC_000062662Source: NYC Law Department, mirrored locally

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