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GCMS analysis report for sample AE07382, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE07382 for unknown compounds and surrogates conducted on April 25, 2002.

NYC-WTC_000061259–000061271

Folder label: “GCMS X 3/28/02 A 4/19/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\041802\7382.D Vial: 31 Acq On : 19 Apr 2002 10:16 am Operator: Bohlk Sample : SAMPLE 7382 3/28/02 Inst : Instrumen Mise : I Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling .: 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading dr trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 9.413 1071 1078 1104 rBV 841471 2698996 58.16% 11.472% 2 10.259 1213 1222 1234 rBV5 ' 20501 67686 1.46% 0.288% 3 12.880 1661 1668 1696 rBV 1783840 4169815 89.85% 17.723% 4 17.986 2529 2537 2560 rBV2 2141784 4641018 100.00% 19.726% 5 19.954 2865 2872 2883 rBV2 146564 310022 6.68% 1.318%

6 22.339 3270 3278 3298 rBV2 1868454 4390968 94.61% 18.663% 7 23.849 3524 3535 3547 rBV3 45394 117986 2.54% 0.501% 8 25.072 3736 3743 3758 rBV2 87729 213844 4.61% 0.909% 9 26.253 3936 3944 3956 rBV2 88048 202957 4.37% 0.863% 10 27.381 4129 4136 4147 rBV3 50251 137536 2.96% 0.585%

11 28.462 4313 4320 4328 rBV3 22885 57793 1.25% 0.246% 12 30.142 4597 4606 4625 rBV2 1592968 3737433 80.53% 15.886% 13 30.765 4705 4712 4721 rBV4 34129 103179 2.22% 0.439% 14 34.014 5255 5265 5282 rBV2 1079509 2677812 57.70% 11.382%

Sum of corrected areas: 23527045

7382.D 5080402BBC.M Tue Apr 23 19:05:11 2002 Page 1

NYC-WTC_000061264

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NYC-WTC_000061264Source: NYC Law Department, mirrored locally

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