GCMS analysis results, sample AE07176, April 25, 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\041802\7176.D Vial: 13 Acq On : 18 Apr 2002 6:40 pm Operator: Bohlk Sample : SAMPLE 7176 3/27/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.512 411 414 441 rBV 158873 474488 7.86% 1.521% 2 9.413 1072 1078 1104 rBV 1362444 3737393 61.90% 11.977% 3 10.259 1215 1222 1234 rBV4 20732 65573 1.09% 0.210% 4 12.885 1661 1669 1691 rBV 2506241 5402453 89.48% 17.313% 5 17.991 2529 2538 2569 rBV 2809155 6037865 100.00% 19.350%

6 19.954 2865 2872 2883 rBV2 181532 400828 6.64% 1.285% 7 22.339 3269 3278 3301 rBV2 2536384 5769436 95.55% 18.489% 8 30.148 4597 4607 4640 rBV2 2147441 5190586 85.97% 16.634% 9 30.765 4705 4712 4734 rBV2 131066 401742 6.65% 1.287% 10 34.020 5252 5266 5287 rBV2 1461069 3723601 61.67% 11.933%

Sum of corrected areas: 31203965

'176.D 5080402BBC.M Tue Apr 23 18:24:42 2002 Page 1 /

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