GCMS analysis results for sample AE06588, April 18, 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\041502\6588.D Vial: 12 Acq On : 15 Apr 2002 7:06 pm Operator: Bohlk Sample : SAMPLE 6588 3/20/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.429 395 400 429 rBV 298101 794546 16.70% 3.199% 2 9.407 1071 1077 1102 rBV 1052023 2876362 60.47% 11.581% 3 10.253 1213 1221 1232 rBV5 18427 62976 1.32% 0.254% 4 12.880 1661 1668 1689 rBV 1950284 4267110 89.71% 17.180% 5 17.986 2528 2537 2557 rBV 2307839 4756457 100.00% 19.151%

6 22.339 3269 3278 3297 rBV2 2054576 4591182 96.53% 18.485% 7 27.275 4112 4118 4130 rBV 299891 565549 11.89% 2.277% 8 30.142 4596 4606 4631 rBV2 1685466 4045550 85.05% 16.288% 9 34.014 5255 5265 5285 rBV2 1173335 2877478 60.50% 11.585%

Sum of corrected areas: 24837210

6588.D 5080402BBC.M Wed Apr 17 17:46:51 2002 Page 1

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