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GCMS surrogate recovery results, sample AE07113, April 16, 2002

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Laboratory report documenting GCMS analysis of surrogates for sample AE07113 on April 16, 2002.

NYC-WTC_000061094–000061102

Folder label: “GCMS X 3/27/02 A 4/11/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\041002\7113.D Vial: 20 Acq On : 11 Apr 2002 5:39 am Operator: Bohlk Sample : SAMPLE 7113 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 9.407 1071 1077 1099 rBV 1031132 2881789 57.03% 11.329% 2 11.922 1498 1505 1520 rBV 129730 240562 4.76% 0.946% 3 12.880 1660 1668 1696 rBV 2095080 4454395 88.14% 17.512% 4 17.985 2529 2537 2561 rBV 2433409 5053502 100.00% 19.867% 5 19.948 2864 2871 2883 rBV2 166822 346755 6.86% 1.363%

6 22.333 3269 3277 3300 rBV2 2104357 4812681 95.23% 18.921% 7 30.136 4596 4605 4627 rBV2 1747441 4169348 82.50% 16.391% 8 30.765 4703 4712 4735 rBV2 116039 315306 6.24% 1.240% 9 34.014 5253 5265 5285 rBV2 1258953 3161889 62.57% 12.431%

Sum of corrected areas: 25436227

'113.D 5080402BB.M Mon Apr 15 18:04:10 2002 Page 1

NYC-WTC_000061099

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NYC-WTC_000061099Source: NYC Law Department, mirrored locally

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