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GCMS analysis results, sample AE06580, April 23, 2002

Machine-extracted title · confidence 95%

GCMS analysis report for sample AE06580 showing surrogate recovery data and unknown compounds.

NYC-WTC_000060804–000060813

Folder label: “GCMS X 3/25/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\O417O2\658O.D Vial: 10 Acq On : 17 Apr 2002 4:06 pm Operator: Bohlk Sample : SAMPLE 6580 3/25/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-me... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.54 0.98.ug/L 58738 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H12O2 000123-42-2 83 2 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H12O2 000123-42-2 74 3 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H12O2 000123-42-2 74 4 3-Oxetanol, 2,2,3-trimethyl-___________ 116 C6H12O2 025910-96-7 23 Abundance Scan 418 (5.535 min): 6580.D (-) m/z 43.10 100.00% 40 59

5000

101 5.20 5.40 5.60 5.80 84 m/z 59.10 68.19% 0 ..................... I ' ' ' ' I ' ' ' 'I' 1,1 I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' m/z-> 20 30 40 50 60 70 80 90 100 110 Abundance #16613: 2-Pentanone, 4-hydroxy-4-methyl- (CAS) $S Diaceton... 4(3

59 5000 , I jnTi.th 101 5.20 5.40 5.60 5.80 m/z 58.10 34.31%

69 83 I m/z—> 20 Ot 30 40 50 I ' ' ‘ 'Y' 60 70 ' 80I'''... 90 ''100 J...110 Abundance #16614: 2-Pentanone, 4-hydroxy-4-methyl- (CAS) $S Diaceton... 4i3

5.20 5.40 5.60 5.80 5000 m/z 101.10 20.77% 59

101 Oiyn ' I ' ' ' ’l'' + " ...... A I Ji... m/z-> 20 30 40 50 60 70 80 90 100 110 Abundance #16610: 2-Pentanone. 4-hydroxy-4-methyl- (CAS) $$ Diaceton... 40 5.20 5.40 5.60 5.80 m/z 41.10 8.62%

5000 28 59

101 I ............... 8,3..........I J, , , , , , 0 m/z-> 20 30 40 50 60 70 80 90 100 110 5.20 5.40 5.60 5.80

6580.D 5080402BBC.M Mon Apr 22 11:04:52 2002 Page 3

NYC-WTC_000060811

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NYC-WTC_000060811Source: NYC Law Department, mirrored locally

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