GCMS sample AE06987 results, April 22, 2002

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Laboratory analysis report for sample AE06987 showing surrogate recovery data and identification of unknown compounds.

NYC-WTC_000060750–000060757

Folder label: “GCMS X 3/25/02 A 4/18/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\APR1802\6986.D Vial: 13 Acq On : 18 Apr 2002 11:41 pm Operator: Sample : GC/MS SCAN 3/25 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 19 9:00 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.21 152 572057 20.00 ug/1 -0.03 10) Naphthalene-d8 15.84 136 2075485 20.00 ug/1 -0.03 17) Acenaphthene-dlO 21.15 164 1154037 20.00 ug/1 -0.02 30) Phenanthrene-dlO 25.58 188 1689663 20.00 ug/1 -0.03 39) Chrysene-dl2 33.64 240 1120948 20.00 ug/1 -0.03 45) Perylene-dl2 37.88 264 746032 20.00 ug/1 -0.04 System Monitoring Compounds 28) TCMX 0.00 209 0 0.00 ug/L Spiked Amount 10.000 Recovery = 0.00% 38) 2,4-DDD 30.66 235 84834 4.31 ug/mL 0.16 Spiked Amount 5.000 Recovery = 86.20% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.48 . 74 311 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 .0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene' 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.63 149 686 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. (#) = qualifier out of range (m) = manual integration 6986.D GCMS0412.M Fri Apr 19 09:02:17 2002 Page 1

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GCMS sample AE06986 results, April 22, 2002 · Box DEP Box 57

NYC-WTC_000060742

Laboratory analysis report for sample AE06986 documenting surrogate recovery and detection of unknown substances.

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