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GCMS Method 508 sample analysis results, April 9 2002

Machine-extracted title · confidence 100%

Gas chromatography mass spectrometry analytical results for environmental samples collected March 18.

NYC-WTC_000060246–000060253

Folder label: “GCMS X 3/18/02 A 4/8/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) s Data File C:\MSDCHEM\l\DATA\020409\6338.D Vial: 7 Acq On 9 Apr 2002 8:45 pm Operator: McLean Sample 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 26 13:29:09 2002 Quant Results File: SCANAPR0©02.R Quant Method : C:\MSDCHEM\1...\SCANAPR0902.M (Chemstation Integrator) .. Title : Method 508 GC/MS Scan , \ 1/ Last Update : Fri Apr 26 13:24:19 2002 j/’ \p h Response via : Initial Calibration . V DataAcq Meth : 508SC7kNl W'i \

Internal Standards • R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 10.66 152 5005049 40.00 ug/1 0.00 10) Naphthalene-d8 15.78 136 18890103 40.00 ug/1 0.00 17) Acenaphthene-dlO 23.67 164 10821792 40.00 ug/1 0.00 30) Phenanthrene-dlO 30.91 188 17492923 40.00 ug/1 0.00 38) Chrysene-dl2 39.10 240 13547885 40.00 ug/1 -0.01 44) Perylene-dl2 x 42.31 264 6791438 40.00 ug/1 0.00 System Monitoring Compounds 27) TCMX 0.00 207 0 .0.00 ug/1 Spiked Amount 4.000 Recovery = 0.00% 37) 2,4-DDD 36.62 235 641270 2.92 ug/ml 0.00 Spiked Amount 4^ Recovery Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 6338.D SCANAPR0902.M Thu May 02 15:07:51 2002 Page 1

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NYC-WTC_000060246Source: NYC Law Department, mirrored locally

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