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GCMS analysis results for sample AE06052, April 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of environmental sample AE06052 conducted on April 11, 2002.

NYC-WTC_000060151–000060159

Folder label: “GCMS X 3/15/02 A 4/6/02

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Scanned page image, NYC-WTC_000060158
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\040502\6052.D Vial: 11 Acq On 6 Apr 2002 4:37 am Operator: Bohllc Sample SAMPLE 6052 3/15/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 3-Buten-2-ol, 2-methyl- Concentration Ranlc 1

R.T. EstConc Area Relative to ISTD R.T.

4.53 0.43 ug/L 231461 1,4-Dichlorobenzene-d4 9.46

Hit# of 5 Tentative ID MW■ MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 43 2 2-METHYLBUT-3-EN-2-OL 86 C5H100 000000-00-0 35 3 3-Penten-2-ol (CAS) $$ 2-PENTEN-... 86 C5H10O 001569-50-2 35 4 Oxirane, propyl- 86 C5H10O 001003-14-1 35 <kbundance Scan 247 (4.531 min): 6052.D (-) m/z 43.10 100.00% 43 TH

5000 55 59 39 67 4.20 4.40 4.60 4.80

m/z-> 0 ....Iillligl. J li3L 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 87 m/z 71.10 98.31%

Abundance #4084: 3-Buten-2-ol. 2-methyi- 7l 43

mill I 'VI . 59 4.20 4.40 4.60 4.80 m/z 69.10 77.57% 27 31 39 53 , 86 67 0; ... ............ . !i'i.......... |l......... I m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4181: 2-METHYLBUT-3-EN-2-OL 43 .................. 4.20 4.40 4.60 4.80 5000 m/z 41.10 71.65%

39 54 86 0 ; y5 I m/z-> 5 .10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4043: 3-Penten-2-ol (CAS) S$ 2-PENTEN-4-OL $$ Methyl prop... 71 43 4.20 4.40 4.60 4.80 m/z 55.10 45.21%

mil 27 39 15 53 31 58 67 86 0 TrrrfTT I HI m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.20 4.40 4.60 4.80

5052.D 5080402.M Mon Apr 08 13:00:51 2002 Page 3

NYC-WTC_000060158

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NYC-WTC_000060158Source: NYC Law Department, mirrored locally

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