GCMS total ion chromatogram data file DFJ0404-D, April 2002

NYC 9/11 Public Portal Document

Response Factor Report Instrumen

Method : C:\MSDCHEM\l\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Fri Apr 05 05:56:22 2002 Response via : Initial Calibration

Calibration Files 6 =C100J404.D 1 =C5J0404.D 2 =C10J0404.D 3 =C25J0404.D 4 =C40J040.D 5 =C80J0404.D

Compound 6 1 2 3 4 • 5 Avg %RSD

1) I 1,4-Dichlorobenzene-d ISTD 2) T N-nitroso-dimet 0.813 0.640 0.716 0.725 0.870 0.815 0.763 11.03 3) bis(2-chloroeth 0.973 1.263 1.221 1.049 1.142 1.020 1.112 10.42 4) 1,3 Dichlorob 0.881 1.180 1.099 0.919 1.037 0.918 1.006 11.85 5) 1,4 Dichlorob 0.865 1.132 1.066 0.910 1.021 0.907 0.983 10.72 6) 1,2 Dichlorob 0.807 1.058 0.990 0.845 0.949 0.840 0.915 10.86 7) 2,2 ' - oxybis 1.416 2.089 1.808 1.594 1.817 1.574 1.716 13.85 8) N-Nitroso-di-n- 0.745 0.925 0.908 0.815 0.869 0.816 0.846 7.94 9) i Hexachloroethan 0.297 0.452 0.433 0.372 0.397 0.315 0.378 16.50

10) Naphthalene-d8 ------------------------------- ISTD-------------------- .--------------- 11) Nitrobenzene 0.301 0.338 0.344 0.290 0.333 0.305 0.318- 7.06 12) Isophorone 0.573 0.568 0.585 0.513 0.621 0.590 0.575 6.22 13) bis(2-Chloroeth 0.331 0.362 0.369 0.326 0.368 0.336 0.348 5.69 14) 1,2,4-Trichloro 0.155 0.197 0.191 0.158 0.176 0.161 0.173 10.37 15) Naphthalene 0.578 0.829 0.781 0.642 0.698 0.614 0.690 14.21 16) Hexachlorobutad 0.079 0.098 0.092 0.078 0.088 0.080 0.086 9.41

17) Acenaphthene-dlO -------------- -ISTD----------------- 18) Hexachlorocyclo 0.123 0.078 0.091 0.099 0.128 0.127 0.107 19.75 19) T 2-chloronaphtha 0.616 0.782 0.746 0.639 0.722 0.635 0.690 9.98 20) I Dimethylphthala 0.744 0.881 0.847 0.729 0.852 0.769 0.804 7.96 21) T 2,6-Dinitrotolu 0.172 0.155 0.174 0.158 0.187 0.174 0.170 6.88 22) Acenaphthylene 0.821 1.022 1.054 0.910 1.008 0.873 0.948 9.85 23) ■ Acenaphthene 0.573 0.808 0.747 0.621 0.683 0.596 0.671 13.72 24) 2,4-Dinitrotolu 0.238 0.200 0.237 0.222 0.263 0.243 0.234 9.04 25) Diethylphthalat 0.562 0.817 0.756 0.636 0.701 0.597 0.678 14.41 26) 4 -Chlorophenyl- 0.313 0.407 0.375 0.322 0.362 0.322 0.350 10.70 27) Fluorene 0.630 0.945 0.875 0.713 0.766 0.660 0.765 16.17 28) Azobenzen/ 1,2- 1.077 1.344 1.300 1.108 1.252 1.158 1.207 8.97

29) Phenanthrene-dlO ------------------------------- ISTD---------------------------------- 30) N-Nitrosodiphen 0.315 0.396 0.385 0.319 0.363 0.328 0.351 10.03 31) 4-Bromophenyl-p 0.115 0.128 0.127 0.107 0.126 0.115 0.120 7.13 32) Hexachlorobenze 0.110 0.128 0.119 0.104 0.118 0.111 0.115 7.60 33) Phenanthrene 0.656 0.862 0.813 0.674 0.750 0.670 0.737 11.59 34) Anthracene 0.648 0.815 0.771 0.664 0.745 0.664 0.718 9.58 35) Di-n-butylphtha 0.761 0.905 0.901 0.781 0.876 0.787 01835 7.88 36) Fluoranthene 0.718 0.810 0.822 0.724 0.803.0.737 0.769 6.16 37) s 2,4-DDD (SURR) 0.187 0.223 0.208 0.200 0.183 0.190 0.199 7.74

38) Chrysene-dl2 ------------------------------- ISTD---------------------------------- 39) Pyrene 1.179 1.217 1.193 1.001 1.229 1.193 1.169 7.21 40) Butylbenzylphth 0.521 0.475 0.510 0.455 0.551 0.526 0.506 6.97 41) Benzo (a) -antra 0.820 0.811 0.796 0.706 0.852 0.821 0.801 6.26 42) Bis (2-ethylhex 0.655 0.618 0.666 0.607 0.706 0.660 0.652 5.48 43) Chrysene 0.755 0.809 0.800 0.673 0.803 0.765 0.767 6.69

44) PerYlene-dl2 ------------------------------- ISTD-------------------- -------------- 45) Di-n-Octylphtha 2.117 1.533 1.855 1.733 2.185 2.078 1.917 13.26 46) Benzo (b) fluor 1.162 1.010 1.034 0.951 1.184 1.147 1.081 8.85 47) Benzo (k) fluor 1.147 1.089 1.229 1.016 1.252 1.159 1.149 7.63

(#) = Out of Range 5080402.M Fri Apr 05 05:58:38 2002 Page 1

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