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GCMS analysis results for sample AE05895, March 29 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of environmental sample AE05895 conducted on March 29, 2002.

NYC-WTC_000059737–000059744

Folder label: “GCMS X 3/13/02 A 3/27/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\MAR2102\5895.D Vial: 23 Acq On : 22 Mar 2002 10:57 am Operator: Sample : gc/ms scan 3/13 Inst : ..GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M {RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.264 780 786 807 rVB 2060437 4541463 67.00% 13.988% 2 15.909 1176 1183 1197 rBV 3046338 6130606 90.45% 18.883% 3 21.215 1754 1761 1775 rBV 3038525 6777843 100.00% 20.876% 4. 25.667 2238 2246 2256 rBV2 3036340 6705913 98.94% 20.655% 5 30.735 2792 2798 2804 rBV 241511 468650 6.91% 1.443%

6 33.728 3111 3124 3142 rBV2 1953391 4657590 68.72% 14.346% 7 37.987 3578 3588 3602 rBV2 1025026 3184332 46.98% 9.808%

Sum of corrected areas: 32466397

5895.D GCMS0308.M Mon Mar 25 14:25:11 2002

NYC-WTC_000059742

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NYC-WTC_000059742Source: NYC Law Department, mirrored locally

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