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GCMS sample analysis with surrogate recovery, Apr 2002

Machine-extracted title · confidence 100%

GCMS analysis of sample AE04516 for organic compounds with surrogate standard 2,4-DDD showing 75% recovery.

NYC-WTC_000058191–000058198

Folder label: “GCMS X 3/2/02 A 3/27/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\MAR2702\4516.D Vial: 7 Acq On : 27 Mar 2002 7:36 pm Operator: Sample : gc/ms scan 3/2 Inst . : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.249 780 785 798 rVB 1614047 3816481 66.66% 14.909% 2 15.885 1175 1181 1199 rBV 2445303 5206053 90.93% 20.337% 3 21.200 1753 1760 1775 rBV 2665546 5725619 100.00% 22.367% 4 25.643 2236 2244 2255 rBV2 2498592 5403723 94.38% 21.109% 5 30.711 2791 2796 2807 rBV 211739 396828 6.93% 1.550%

6 33.704 3113 3122 3141 rBV 1334580 3100628 54.15% 12.112% 7 37.945 3575 3584 3596 rBV2 645040 1949595 34.05% 7.616%

Sum of corrected areas: 25598927

4516.D GCMS0308.M Fri Mar 29 12:56:07 2002

NYC-WTC_000058196

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NYC-WTC_000058196Source: NYC Law Department, mirrored locally

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