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Laboratory method sheet for liquid-liquid extraction parameters

Machine-extracted title · confidence 90%

Technical record detailing laboratory method parameters including drip rates and reagent volumes for sample processing.

NYC-WTC_000059589–000059598

Folder label: “GCMS X 3/12/02 A 4/4/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\APRO3 02\LBA.D Vial: 15 Acq On 4 Apr 2002 8:27 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge .< 100 prefer < Baseline drop else tangent > • Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area ■ % max. total

1 8.129 332 336 363 rVB 94796 264869 6.93% 1.547% 2 12.251 779 785 806 rVB 1011982 2612111 68.38% 15.257% 3 14.840 1063 1067 1072 rVB 19772 39217 1.03% 0.229% 4 15.886 1175 1181 1197 rBV 1550548 3345923 87.59% 19.543% 5 21.183 1752 1758 1774 rBV 1803555 3820135 100.00% 22.312%

6 25.627 2236 2242 2254 rBV2 1604143 3560000 93.19% 20.793% 7 25.774 2254 2258 2270 rVB 11687 39304 1.03% 0.230% 8 30.703 2790 2795 2803 rVB 168776 321537 8.42% 1'. 878% 9 33.687 3112 3120 3134 rBV2 875020 1940937 50.81% 11.336% 10 37.928 3574 3582 3596 rBV2 396862 1177118 30.81% 6.875%

Sum of corrected areas: 17121151

LBA.D GCMS0408.M Tue Apr 16 08:15:32 2002

NYC-WTC_000059593

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NYC-WTC_000059593Source: NYC Law Department, mirrored locally

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