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Document / 9 pages

GCMS blank analysis results, April 2002

Machine-extracted title · confidence 90%

Instrument calibration record using DFTPP standard to verify GCMS performance for analytical testing on April 1, 2002.

NYC-WTC_000059478–000059486

Folder label: “GCMS X 3/12/02 A 4/2/02

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Scanned page image, NYC-WTC_000059482
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File C:\HPCHEM\1\DATA\APRO102\LBA.D Vial: 16 Acq On 2 Apr 2002 3:07 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.134 332 336 362 rVB 112174 294607 7.05% 1.550% 2 12.246 779 784 800 rVB 1238784 2846927 68.17% 14.983% 3 15.882 1174 1180 1197 rBV 1757178 3667346 87.82% 19.301% 4 21.188 1752 1758 1773 rBV 1995140 4175938 100.00% 21.978% 5 25.631 2236 2242 2254 rBV2 1793781 3904486 93.50%' 20.549%

6 30.708 2790 2795 2803 rBV 188751 369809 8.86% 1.946% 7 33.407 3081 3089 3097 rVB3 . 13643 45718 1.09% 0.241% 8 33.692 3113 3120 3137 rBV2 1000645 2258032 54.07% 11.884% 9 37.933 3575 3582 3595 rBV2 471520 1437949 34.43% 7.568%

Sum of corrected areas: 19000812

LBA.D GCMS0403.M Fri Apr 05 10:41:45 2002

NYC-WTC_000059482

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NYC-WTC_000059482Source: NYC Law Department, mirrored locally

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