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GCMS analysis results for sample AE05747, April 11 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05747 conducted on April 11, 2002, including surrogate recovery data.

NYC-WTC_000059576–000059584

Folder label: “GCMS X 3/12/02 A 4/2/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

■ Data File C:\HPCHEM\1\DATA\APR0102\5748.D Vial: 27 Acq On 3 Apr 2002 2:58 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCIjP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.129 332 336 349 rBV 87390 246633 5.96% 1.325% 2 12.251 779 785 800 rVB 1076781 2779577 67.16% 14.930% 3 15.886 1174 1181 1198 rBV 1755997 3646458 88.11% 19.586% 4 21.193 1752 1759 1775 rBV 1994857 4138649 100.00% 22.230% 5 25.636 2236 2243 2254 rBV 1804866 3840595 92.80% 20.629%

6 30.703 2790 2795 2803 rBV 198993 387366 9.36% 2.081% 7 33.687 3113 3120 3141 rBV2 944198 2193404 53.00% 11.781% 8 37.928 3574 3582 3599 rBV2 453523 1384918 33.46% 7.439%

Sum of corrected areas: . 18617600

5748.D GCMS0403.M Fri Apr 05 10:40:09 2002

NYC-WTC_000059581

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NYC-WTC_000059581Source: NYC Law Department, mirrored locally

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