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GC/MS analysis sample AE05745, April 2002

Machine-extracted title · confidence 75%

Gas chromatography/mass spectrometry analysis of sample AE05745 performed April 11, 2002, with surrogate recovery data for 2,4-DDD.

NYC-WTC_000059545–000059554

Folder label: “GCMS X 3/12/02 A 4/2/02

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Scanned page image, NYC-WTC_000059550
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

‘ Data File C:\HPCHEM\l\DATA\APR0102\5745 .D Vial: 24 Acq On 2 Apr 2002 11:59 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing- : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.131 332 336 345 rBV 99062 232831 5.45% 1.198% 2 12.244 779 784 798 rBV 1171915 2862676 66.96% 14.728% 3 15.879 1174 1180 1197 rBV 1742401 3763671 88.04% 19.364% 4 21.185 1752 1758 1772 rBV 1956895 4275185 100.00% 21.996% 5 25.629 2236 2242 2253 rBV2 1804159 3997416 93.50% 20.566%

6 30.705 2790 2795 2806 rVB 214757 412478 9.65% 2.122% 7 33.322 3076 3080 3091 rBV2 28574 60733 1.42% 0.312% 8 33.689 3113 3120 3138 rBV2 1031929 2325053 54.38% 11.962% 9 37.930 3574 3582 3598 rBV 500843 1506526 35.24% 7.751%

Sum of corrected areas: 19436569

5745.D GCMS0403.M Fri Apr 05 10:37:32 2002

NYC-WTC_000059550

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NYC-WTC_000059550Source: NYC Law Department, mirrored locally

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