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GCMS calibration data for sample AE05701, April 2002

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Calibration data sheet listing retention times and response factors for multiple organic compounds analyzed on April 5, 2002.

NYC-WTC_000059491–000059498

Folder label: “GCMS X 3/12/02 A 4/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APRO102\REFA1.D Vial: 17 Acq On : 2 Apr 2002 4:07 am Operator: Sample : gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P ' Quant Time: Apr 5 10:04 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.22 168 156556 6.78 ug/1 # 78 31) 4-Bromophenyl-phenylether 24.29 248 99432 7.32 ug/1 91 32) Hexachlorobenzene 24.73 284 109272 6.93 ug/l # 84 3 3) Phenanthrene 25.70 178 572546 7.75 ug/1 99 34) Anthracene 25.83 178 • 518474 7.08 ug/1 98 35) Di-n-butylphthalate 27.60 149 789322 8.49 ug/1 99 36) Fluoranthene 29.32 202 547219 7.06 ug/1 # 92 39) Pyrene 30.00 202 562807 10.65 ug/1 # 94 40) Butylbenzylphthalate 32.13 149 244318 8.97 ug/1 97 41) Benzo(a)anthracene 33.64 228 333244 7.58 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 304878 8.29 ug/1 # 95 43) Chrysene 33.76 228 364546 8.46 ug/1 99 45) Di-n-Octylphthalate 35.65 149 339779 7.61 ug/1 # 98 46) Benzo(b)fluoranthene 36.75 252 254360 8.22 ug/1 98 47) Benzo(k)fluoranthene 36.81 252 273910m 9.08 ug/1 48) Benzo(a)pyrene 37.74 252 173261 6.14 ug/1 # 96 .49) Indeno (1,2,3-cd) pyrene 42.05 276 169835 4.99 ug/1 96 50) Dibenz(a,h)anthracene 42.13 278 146532 5.56 ug/1 98 51) Benzo(g,h,i)perylene 43.28 276 152676 5.49 ug/1 95

(#) = qualifier out of range (m) = manual integration REFAl.D GCMS0403.M Fri Apr 05 10:04:51 2002 Page 2

NYC-WTC_000059497

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