GCMS calibration data for sample AE05701, April 2002

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Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR0102\REFAl. D Vial: 17 Acq On 2 Apr 2002 4:07 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 5 10:04 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 565866 20.00 ug/1 -0.11 10) Naphthalene-d8 15.88 136 2073077 20.00 ug/1 -0.12 17) Acenaphthene-dlO 21.20 164 1187357 20.00 ug/1 -0.12 29) Phenanthrene-dlO 25.64 188 1710367 20.00 ug/1 -0.13 38) Chrysene-dl2 33.70 240 920020 20.00 ug/1 -0.14 44) Perylene-dl2 37.94 264 506857 20.00 ug/1 -0.18

System Monitoring Compounds 37) 2,4-DDD 30.71 235 79586 4.64 ug/mL 0.21 Spiked Amount 5.000 Recovery = 92.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.89 74 92172 4.80 ug/1 # 66 3) bis(2-Chloroethyl)ether 11.64 93 215072 6.96 ug/1 92 4) 1,3-Dichlorobenzene 12.14 146 79182 2.48 ug/1 99 5) 1,4-Dichlorobenzene 12.29 146 90879 2.84 ug/1 98 6) 1,2-Dichlorobenzene 12.81 146 105315 3.53 ug/1 98 7) 2,2'-oxybis(1-Chloropropan 13.13 45 294364 6.77 ug/1 98 8) N-Nitroso-di-n-propylamine 13.51 70. 147680 7.34.ug/1 # 85 9) Hexachloroethane 13.66 117 10638 0.89 ug/1 91 11) Nitrobenzene 13.93 77 192398 6.79 ug/1 94 12) Isophorone 14.58 82 415714 7.73 ug/1 98 13) bis(2-Chloroethoxy)methane 15.26 93 263887 7.50 ug/1 97 14) 1,2,4-Trichlorobenzene 15.77 180 95318 3.92 ug/1 97 15) Naphthalene 15.95 128 486505 6.35 ug/1 99 16) Hexachlorobutadiene 16.49 225 5783 0.48 ug/1 94 18) Hexachlorocyclopentadiene 18.68 237 2795 0.35 ug/1 95 19) 2-Chloronaphthalene 19.44 162 307419 6.03 ug/1 95 20) Dimethylphthalate 20.54 163 478735 8.01 ug/1 99 21) 2,6-Dinitrotoluene 20.75 165 96877 6.68 ug/1 # 81 22) Acenaphthylene 20.72 152 527932 7.24 ug/1 99 23) Acenaphthene 21.28 153 354412 6.96 ug/1 98 24) 2,4-Dinitrotoluene. 21.92 165 119220 6.14 ug/1 # 76 25) Diethylphthalate 22.67 149 463783 8.00 ug/1 96 26) 4-Chlorophenyl-phenylether 22.82 204 181314 7.30 ug/1 93 27) Fluorene 22.80 166 408343 7.58 ug/1 .99 28) Azobenzen/ 1,2-Diphenylhyd 23.29 77 382601 6.15 ug/L # 82

(#) = qualifier out of range (m) = manual integration REFAl.D GCMS0403.M Fri Apr 05 10:04:48 2002 Page 1

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