GCMS unknown compound analysis, sample AE05515, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

‘ Data File C:\HPCHEM\l\DATA\APR0102\5515.D Vial: 6 ■ Acq On 1 Apr 2002 4:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 2 8:45 2002 Quant Results File: GCMS0308.RES

. Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 622568 20.00 ug/1 -0.10 10) Naphthalene-d8 15.88 136 2329665 20.00 ug/1 -0.11 17) Acenaphthene-dlO 21.20 164 1299749 20.00 ug/1 -0.11 29) Phenanthrene-dlO 25.63 188 1839885 20.00 ug/1 -0.13 38) Chrysene-dl2 33.69 240 927725 20.00 ug/1 -0.15 44) Perylene-dl2 37.94 264 507719 20.00 ug/1 -0.18

System Monitoring Compounds 37) 2,4-DDD 30.71 235 82965 4.49 ug/mL 0.21 Spiked Amount 5.000 Recovery = 89.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.29 146 184 N.D. 5) 1,4-Dichlorobenzene 12.29 146 184 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9)- Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone .0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.93 128 284 N.D. 16) Hexachlorobutadiene 16.49 225 196 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene ■ (

0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.55 165 187 N.D. 25) Diethylphthalate 22.67 149 573 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 5515.D GCMS0403.M Thu Apr 04 12:43:52 2002 Page 1

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