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GCMS unknown compound analysis, sample AE05518, April 2002

Machine-extracted title · confidence 100%

Laboratory record of gas chromatography mass spectrometry analysis for unknown compounds and surrogates on April 10, 2002.

NYC-WTC_000059296–000059306

Folder label: “GCMS X 3/11/02 A 4/1/02

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Scanned page image, NYC-WTC_000059301
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

bata File C:\HPCHEM\1\DATA\APRO102\5518.D Vial: 9 'Acq On 1 Apr 2002 8:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P 1

Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.133 331 336 344 rBV 189962 463440 10.58% 2.266% 2 8.225 344 346 350 rW 38119 93162 2.13% 0.456% 3 8.280 350 352 364 rVB2 23766 63834 1.46% 0.312% 4 12.246 779 784 801 rVB 1235441 2979237 68.04% 14.569% 5 15.881 1174 1180 1197 rBV 1864377 3892235 88.89% 19.034%

6 21.187 1752 1758 1775 rBV 2026741 4378743 100.00% 21.413% 7 25.640 2236 2243 2254 rBV 1849882 4060022 92.72% 19.854% 8 30.707 2790 2795 2802 rBV 216060 425864 9.73% 2.083% 9 33.691 3113 3120 3135 rBV2 1058135 2451756 55.99% • 11.990% 10 37.941 3573 3583 3603 rBV2 544583 1640816 37.47% 8.024%

Sum of corrected areas: 20449109

5518.D GCMS0403.M Thu Apr 04 13:55:36 2002

NYC-WTC_000059301

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NYC-WTC_000059301Source: NYC Law Department, mirrored locally

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