GCMS unknown compound analysis, sample AE05698, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APR0102\5698.D Vial: 13 Acq On 2 Apr 2002 12:09 am Operator: I Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD • R.T.

8.13 3.28 ug/1 463486 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, t^ramethyl- 88 C4H12Si 000075-76-3 9 2 1,3-Diox<^ane, 2-pentadecyl- 284 C18H36O2 004360-57-0 9 3 Butane, /-methoxy-2-methyl- 102 C6H14O 000994-05-8 9 4 1 - But aiy mine. 3-methyl- 87 C5H13N _________ 000107-85-7 7 Abundance Scan 336 (8,127 min): 5698.D (-) m/z' 73.00“ 100.00% 1 73

5000 43 7,80 8.00 8.20 8.40 ,1.1 57 87 103 prr-r-T-p-r-n-r m/z 43.05 28.2.3% ni/z-> . 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #62932: Silane, tetramethyl- I 7(3

5000 7.80 8.00 8.20 i8.40 45 m/ z 10.41% 15 , J, .88............... ,,,, ,,,, ........... - 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #40191; 1.3-Dioxolane, 2-Deiitadecvl- i 73 i ' 7,80 ' '' p-i ' I 8.00 8.20 I8.40 5000 m/z 45.05 10.26%

43 ^7 86.99...................................................................... 256 283 m/z-> 20 40 60 8o_..JJoZi2oZj4g_i6gZi8y3^ pKbundance #1761: Butane. 2-methoxy-2-methyl- ...... I 7(3 7.80 m/z 8.00 8.20 8.40 6.31% 5000 55 87

I T-jL-r rm-n-r,- '' I'' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 7.80 8.00 8.20 8.40

5698.D GCMS0403.M Thu Apr 04 13:58:40 2002 Page 1

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