Reference standard analysis report for volatile organic compounds using GCMS on April 4, 2002.
NYC-WTC_000059222–000059229Folder label: “GCMS X 3/11/02 A 4/1/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\APRO102\REF2.D Vial: 5 Acq On 1 Apr 2002 3:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 4 12:39 2002 Quant Results File: GCMS0308.RES
•Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 23.22 168 133359 5.69 ug/1 # 80 31) 4-Bromophenyl-phenylether 24.29 248 107360 7.79 ug/1 93 32) Hexachlorobenzene 24.73 284 126903 ■ 7.93 ug/1 # 87 3 3) Phenanthrene 25.70 178 566662 7.56 ug/1 99 34) Tknthracene 25.83 178 506187 6.81 ug/1 98 35) Di-n-butylphthalate 27.60 149 713591 7.56 ug/1 .# 98 36) Fluoranthene 29.33 202 541880 6.89 ug/1 96 3 9) Pyrene 30.00 202 545773 10.13 ug/1 # 91 40) Butylbenzylphthalate 32.13 149 235183 8.46 ug/1 98 4i) Benzo(a)anthracene 33.65 228 319412 7.13 ug/1 98 42) Bis(2-ethylhexyl)phthalate 33.91 149 283359 7.55 ug/1 94 43) Chrysene 33.77 228 340626 7.75 ug/1 100 45) Di-h-Octylphthalate 35.66 149 330941 7.23 ug/1 # 96 46) Benzo(b)fluoranthene 36.75 252 241123m 7.60 ug/1 47) Benzo(k)fluoranthene 36.82 252 267799m 8.66 ug/1 48) Benzo(a)pyrene 37.74 252 144782 5.01 ug/1 # 94 49) Indeno(1,2,3-cd)pyrene 42.06 ■ 276 165319 4.74 ug/1 98 50) Dibenz(a,h)anthracene 42.13 278 143871 5.32 ug/1 97 51) Benzo(g,h,i)perylene 43.30 276 146431 5.14 ug/1 96
(#) = qualifier out of■range (m) = manual integration REF2.D GCMS0403.M Thu Apr 04 12:41:06 2002 Page 2
NYC-WTC_000059228
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NYC-WTC_000059491
Calibration data sheet listing retention times and response factors for multiple organic compounds analyzed on April 5, 2002.
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Reference standard analysis report for sample AE04733 conducted April 1, 2002, listing concentrations of quality control compounds.
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Laboratory report listing concentrations of target analytes in a reference standard analyzed on March 29, 2002.
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Quantitative results for reference standards analyzed by GCMS on April 3, 2002, to validate analytical accuracy.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059118
Calibration results for specific volatile organic compounds used to verify GCMS instrument performance in April 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058498
Laboratory report listing concentrations of target analytes in a reference standard analyzed on April 2, 2002.
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Reference standard analysis for gas chromatography-mass spectrometry dated March 29, 2002.
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DEP laboratory report of GCMS reference analysis for sample AE06633 conducted on April 17, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010289
Reference data report displaying measured concentrations and detection limits for target analytes analyzed on March 21, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048709
Calibration table listing results for various organic compounds including nitrosamines and dichlorobenzenes from April 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049000
Reference standard analysis for GCMS testing of volatile organic compounds conducted on April 23, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012309
Laboratory report for GC/MS reference analysis of sample AE04417 conducted on March 22, 2002.
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Blank quality control GCMS analysis of sample AE05515 conducted April 4, 2002, showing below-detection-limit results for sixteen organic compounds.
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Calibration data for gas chromatography mass spectrometry analysis of volatile organic compounds dated April 4, 2002.
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Laboratory record of gas chromatography mass spectrometry analysis for unknown compounds and surrogates on April 9, 2002.
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