GCMS reference standard results, sample AE05515, April 2002

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Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR0102\REF2.D Vial: 5 Acq On 1 Apr 2002 3:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 4 12:39 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title •: 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 567883 20.00 ug/1 -0.10 10) Naphthalene-d8 15.89 136 2117435 20.00 ug/1 -0.11 17) Acenaphthene-dlO 21.20 164 1192766 20.00 ug/1 -0.12 29) Phenanthrene-dlO 25.64 188 1735696 20.00 ug/1 -0.13 38) Chrysene-dl2 33.70 240 938406 • 20.00 ug/1 -0.14 44) Perylene-dl2 37.94 264 519313 20.00 ug/1 -0.18

System Monitoring Compounds 37) 2,4-DDD 30.71 235 80762 4.64 ug/mL 0.21 Spiked Amount 5.000 Recovery = 92.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine .5.89 74 88714 4.60 ug/1 # 67 3) bis (2-Chloroethyl) ether. 11.64 93 210480 ■6.78 ug/1 92 4) 1,3-Dichlorobenzene 12.15 146 179539 5.60 ug/1 98 5) 1,4-Dichlorobenzene 12.29 146 190316 5.92 ug/i 97 6) 1,2-Dichlorobenzene 12.82 146 184961 6.17 ug/1 97 7) 2,2'-oxybis(1-Chloropropan 13.13 45 297753 6.82 ug/1 100 8) N-Nitroso-di-n-propylamine 13.51 70 140845 6.98 ug/1 # 87 9) Hexachloroethane 13.66 117 60037 5.00 ug/1 96 11) Nitrobenzene 13.94 77 192210 .6.64 ug/1 91 12) Isophorone 14.58 82 416950 7.60 ug/1 99 13) bis(2-Chloroethoxy)methane 15.26 93 260261 7.24 ug/1 97 14) 1,2,4-Trichlorobenzene 15.77 180 160736 6.47 ug/1 96 15) Naphthalene 15.95 128 563014 7.19 ug/1 99 16) Hexachlorobutadiene 16.49 225 66814 5.39 ug/1 97 . 18) Hexachlorocyclopentadiene 18.68 237 9673 1.20 ug/1 97 19) 2-Chloronaphthalene 19.44 162 338608 6.61 ug/1 96 20) Dimethylphthalate 20.54 163 453213 7.55 ug/1 99 21) 2,6-Dinitrotoluene 20.76 165 92898 6.38 ug/1 # • 80 22) Acenaphthylene 20.72 152 515398 7.04 ug/1 99 23) Acenaphthene 21.29 153 365404 7.14 ug/1 98 24) 2,4-Dinitrotoluene 21.92 165 119828 6.15 ug/i # 76 25) Diethylphthalate 22.67 149 436614 7.49 ug/1 96 26) 4-Chlorophenyl-phenylether 22.82 204 198174 7.94 ug/1 92 27) Fluorene 22.80 166 407431 ■7.53 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.29 .. 77 378574 6.06 ug/L # 84

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0403.M Thu Apr 04 12:41:02 2002 Page 1

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