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GCMS analysis results, sample AE05237, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE05237 for unknown compounds on April 9, 2002.

NYC-WTC_000059196–000059206

Folder label: “GCMS X 3/9/02 A 3/30/02

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Scanned page image, NYC-WTC_000059202
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

■ Data File C:\HPCHEM\l\DATA\MAR3002\5237.D Vial: 48 Acq On 31 Mar 2002 3:35 pm Operator: Sample gc/ms scan 3/9 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.140 333 337 348 rBV 22979 62056 1.79% 0.390% 2 12.244 779 784 805 rVB 931043 2362402 68.20% 14.842% 3 14.842 1063 1067 1076 rVB 19187 37910 1.09% 0.238% 4 15.889 1174 1181 1198 rBV 1406125 3038286 87.71% ■ 19.088% 5 21.195 1752 1759 1770 rBV 1626733 3464048 100.00% 21.763%

6 25.629 2236 2242 2254 rBV2 1487199 3226403 93.14% 20.270% 7 30.706 2790 2795 2801 rBV 228736 434593 12.55% 2.730% 8 33.689 3114 3120 3133 rBV2 850736 1921562 55.47% 12.072% 9 33.910 3139 3144 3151 rVB 19845 45950 1.33% 0.289% 10 37.940 3575 3583 3602 rBV2 428989 1324011 38.22% 8.318%

Sum of corrected areas: 15917221

5237.D GCMS0308.M Wed Apr 03 14:03:10 2002

NYC-WTC_000059202

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NYC-WTC_000059202Source: NYC Law Department, mirrored locally

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