GCMS analysis results, sample AE05235, April 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report I I

• Data File : C:\HPCHEM\l\DATA\MAR3002\5235.D Vial: 46 Acq On : 31 Mar 2002 1:36 pm Operator: Sample : gc/ms scan 3/9 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method - : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table 1 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 I

Signal : TIC

peak R.T. first max last PK peak peak peak % of I I # min scan scan scan TY height area % max. total

1 8.142 332 337 346 rBV 32971 86252 2.36% 0.512% 2 11.878 739 744 749 rBV 18545 41552 1.14% 0.247% 3 11'. 961 749 753 764 rVB 21542 ■ 52415 1.44% 0.311% 4 12.181 772 777 780 rBV 33728 78867 2.16% 0.469% 5 12.246 780 784 799 rVB 972538 2448712 67.10% 14.548% I I 6 14.844 1063 1067 1072 rVB 28189 55067 1.51% 0.327% 7 15.881 1174 1180 1198 rBV 1481684 3182232 87.20% 18.905% 8 21.187 1752 1758 1774 rBV 1755500 3649208 100.00% 21.680% 9 25.631 2236 2242 2254 rBV2 1574897 3377104 92.54% 20.063% 10 30.707 2790 2795 2804 rBV 243115 468350 12.83% 2.782%

11 33.691 3113 3120 3139 rBV2 896205 2031312 55.66% 12.068% 12 37.932 3574 3582 3596 rBV2 448276 1361428 37.31% 8.088% 1 Sum of corrected areas: 16832499 I 5235.D GCMS0308.M Wed Apr 03 14:00:56 2002

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