GCMS sample header with drip rate data, March 2002

NYC 9/11 Public Portal Document

DFTPP

Data File C:\HPCHEM\l\DATA\MAR2602\DFTPP.D Vial: 1 Acq On 26 Mar 2002 8:44 am Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP.D 4000000-

. 3000000- i 1 ' 2000000

1 ' 1000000

;Time-> 04 ............i.L,. ... aA................ 25.00 25.20 25.40 25.60 25.80 26.00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27.60 27.80 28.00 28.20 28.40 28.60 Average of 26.805 to 26.869 min.: DFTPP.D Abundance 198 200000 442

150000

69 127 255 100000 ! 51 110 275 50000 224 ,1 24j2 , _ 2^^310323336 352365 333 403 423 . 0 3g ' ‘1'' W-f-v ........... . 1. _____________________________ :• m/z--> 40 60 8L J102 120 J40 J60 JM 200L^P 24^260 280 300 320 3^360 380 40g.^2^0

Spectrum Information: Average of 26.805 to 26.869 min.

I Target Rei. to I Lower Upper Rei. Raw I Result I Mass Mass I Limit% Limit% Abn% Abn i Pass/Fail

' 51 198 30 60 35.3 78897 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 46.7 104438 PASS 70 69 0.00 2 0.0 0 PASS 127 198 40 60 42.9 95766 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 223469 PASS 199 198 5 9 6.8 15088 PASS 275 198 10 30 22.8 50955 ■PASS 365 198 1 . 100 2.4 5350 PASS 441 443 0.01 100 98.1 32294 PASS 442 198 40 110 76.6 171182 PASS 443 442 17 23 19.2 32936 PASS

DFTPP.D GCMS0308.M Fri Mar 29 09:49:34 2002

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