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GCMS analysis results for sample AE04805, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE04805 conducted on April 5, 2002.

NYC-WTC_000058523–000058536

Folder label: “GCMS X 3/5/02 A 3/29/02

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Scanned page image, NYC-WTC_000058528
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File C:\HPCHEM\1\DATA\MAR2 802\4805.D Vial: 20 Acq On 29 Mar 2002 3:23 am Operator: Sample gc/ms scan 3/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P.

Method' : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.250 780 785 804 rVB 963492 2240484 67.40% 14.660% 2 15.885 1175 1181 1199 rBV 1406431 2883349 86.74% 18.866% . 3 21.191 1753 1759 1775 rBV 1626097 3324242 100.00%. 21.751% 4 25.635 2237 2243 2254 rBV2 1470804 3032770 91.23% 19.844% 5 30.711 2791 2796 2801 rBV 227192 433126 13.03% 2.834%

6 33.695 3114 3121 3136 rBV 771687 1728252 51.99% 11.308% 7 36.137 3383 3387 3396 rBV2 15423 44759 1.35% 0.293% 8 37.376 3515 3522 3536 rBV 23260 85520 2.57% 0.560% 9 37.936 3576 3583 3598 rBV2 379633 1115573 33.56% 7.299% 10 38.827 3672 3680 3696 rBV2 23825 103036 3.10% 0.674%

11 40.580 3863 3871 3882 rBV5 20512 106287 3.20% 0.695% 12 42.765 4099 4109 4122 rBV4 16715 98174 2.95% 0.642% 13 45.547 4398 4412 4422 rBV7 11488 87635 2.64% 0.573%

Sum of corrected areas: 15283207

4805.D GCMS0308.M Mon Apr 01 15:49:08 2002

NYC-WTC_000058528

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NYC-WTC_000058528Source: NYC Law Department, mirrored locally

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