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GCMS sample analysis with surrogate recovery, Apr 2002

Machine-extracted title · confidence 100%

GCMS analysis of sample AE04416 for organic compounds with surrogate standard showing 5.0 micrograms detection limit.

NYC-WTC_000058183–000058190

Folder label: “GCMS X 3/2/02 A 3/27/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2702\4416.D Vial: 6 Acq On : 27 Mar 2002 6:36 pm Operator: San^ile : gc/ms scan 3/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 29 12:38 2002 Quant Results File: GCMS0308.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.70 178 1143 N.D. 34) Anthracene 25.83 178 733 N.D. 35) Di-n-butylphthalate 27.60 149 100973 0.73 ug/1 # 97 36) Fluoranthene 29.33 202 773 N.D. 39) Pyrene 30.00 202 823 N.D. 40) Butylbenzylphthalate 32.13 149 981 N.D. 41) Benzo(a)anthracene 33.77 228 2734 N.D. 42) Bis{2-ethylhexyl)phthalate 33.92 149 5221 N.D. 43) Chrysene 33.77 228 2914 N.D. 45) Di-n-Octylphthalate 35.66 149 947 N.D. 46) Benzo(b)fluoranthene 36.75 252 1450 N.D. 47) Benzo(k)fluoranthene 36.82 252 2072 N.D. 4 8) Benzo(a)pyrene 37.74 252 1131 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 43.33 276 100 N.D.

{#) = qualifier out of range (m) = manual integration 4416.D GCMS0308.M Fri Mar 29 12:39:12 2002 Page 2

NYC-WTC_000058186

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NYC-WTC_000058186Source: NYC Law Department, mirrored locally

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