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GCMS analysis results, sample AE04948, March 2002

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Laboratory report detailing quantitative results for volatile organic compounds in sample AE04948 analyzed on March 29, 2002.

NYC-WTC_000058735–000058743

Folder label: “GCMS X 3/7/02 A 3/27/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2602\4948.D Vial: 20 Acq On : 27 Mar 2002 4:33 am Operator: Sample : gc/ms scan 3/7 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 29 11:46 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.70 178 847 N.D. 34) Anthracene 25.83 178 371 N.D. 35) Di-n-butylphthalate 27.60 149 2832 N.D. 36) Fluoranthene 29.33 202 227 N.D. 3 9) Pyrene 30.00 202 398 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.69 228 3455 N.D. 42) Bis(2-ethylhexyl)phthalate 33.91 149 11707 0.28 ug/1 100 43) Chrysene 33.77 228 1436 N.D. 45) Di-n-Octylphthalate 35.66 149 345 N.D. 46) Benzo(b)fluoranthene 36.74 252 466 N.D. 47) Benzo(k)fluoranthene 36.82 252 600 N.D. 48) Benzo(a)pyrene 37.75 252 279 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 ■ N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 4948.D GCMS0308.M Fri Mar 29 11:46:59 2002 Page 2

NYC-WTC_000058738

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NYC-WTC_000058738Source: NYC Law Department, mirrored locally

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