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Analytical results for sample AD28308 using Method 525.2, Dec 2001

Machine-extracted title · confidence 100%

Lab report listing analytical results for multiple compounds in sample AD28308 with detection limits on December 18, 2001.

NYC-WTC_000058131–000058135

Folder label: “525 X 11/26/01 A 12/14 - 12/15/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\121401\28308.D vial: 15 Acq On : 15 Dec 2001 3:19 am Operator: McLean Sample : 11/26/01 525 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 18 09:44:50 2001 Quant Results File: 121401.RES

Quant Method : C:\MSDCHEM\l\5973N\121401.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Tue Dec 18 09:35:41 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 18.20 164 6413240 5.00 ug/L 0.00 9) Phenanthrene D-10 22.53 188 9796878 5.00 ug/L 0.00 20) Chrysene D-12 30.30 240 6872741 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.13 134 1653299 5.04 ug/L 0.00 Spiked Amount 5.000 Recovery = 100.80% 19) Triphenyl Phosphate surr 29.58 326 1726063 5.79 ug/L 0.00 Spiked Amount 5.000 Recovery = 115.80% 21) Perylene D-12 surr 34.31 264 5023085 5.53 ug/L 0.00 Spiked Amount 5.000 Recovery = 110.60%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. d 4) Hexachlorobenzene 21.40 284 21256 0.05 ug/L 88 5) EPTC 0.00 12 8 0 N.D. 6) 2,6-Dinitrotoluene 17.82 165 18448 0.36 ug/L # 30 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 0.00 126 0 N.D. d 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. d 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 27.29 246 13665 0.04 ug/L 81 22) Bis (2-Ethylhexyl) adipate 29.51 129 28764 0.41 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 30.96 149 321732 0.53 ug/L 95 24) Benzo (a) pyrene 34.16 252 11883 0.01 ug/L # 63

(#) = qualifier out of range (m) = manual integration 28308.D 121401.M Tue Dec 18 09:47:39 2001 Page 1

NYC-WTC_000058132

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NYC-WTC_000058132Source: NYC Law Department, mirrored locally

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