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Reference standard results for sample AD28048, Dec 2001

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Lab record of reference standard analysis for sample AD28048 using Method 525.2 on December 18, 2001.

NYC-WTC_000058123–000058126

Folder label: “525 X 11/26/01 A 12/14 - 12/15/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\121401\28048.D Vial: 14 * Acq on : 15 Dec 2001 2:34 am Operator: McLean Sample : 11/26/01 525 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 18 09:41:20 2001 Quant Results File: 121401.RES

Quant Method : C:\MSDCHEM\l\5973N\121401.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Tue Dec 18 09:35:41 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.20 164 5649454 5.00 ug/L 0.00 9) Phenanthrene D-10 22.53 188 8478731 5.00 ug/L 0.00 20) Chrysene D-12 30.30 240 5359429 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.13 134 1423891 4.93 ug/L 0.00 Spiked Amount 5.000 Recovery = 98.60% 19) Triphenyl Phosphate surr 29.58 326 1440344 5.58 ug/L 0.00 Spiked Amount 5.000 Recovery = 111.60% 21) Perylene D-12 surr 34.31 264 3520163 4.97 ug/L 0.00 Spiked Amount 5.000 Recovery = 99.40%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 18.94 165 1378 0.31 ug/L # 21 8) Molinate 18.98 126 11715 0.02 ug/L # 1 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 161 0 N.D. d 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.51 129 15026 0.40 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 30.96 149 226044 0.51 ug/L 93 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 28048.D 121401.M Tue Dec 18 09:42:04 2001 Page 1

NYC-WTC_000058124

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NYC-WTC_000058124Source: NYC Law Department, mirrored locally

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