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Calibration standard results, sample AD28048, Dec 2001

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Calibration standard analysis results for sample AD28048 showing pesticide compound responses on December 18, 2001.

NYC-WTC_000058116–000058118

Folder label: “525 X 11/26/01 A 12/14 - 12/15/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\121401\CAL5A.D Vial: 6 Acq On 14 Dec 2001 8:34 pm Operator: McLean Sample 1.0 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 18 11:11:56 2001 Quant Results File: 121401.RES

Quant Method : C:\MSDCHEM\l\5973N\121401.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Tue Dec 18 09:35:41 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.20 164 8189928 5.00 ug/L 0.00 9) Phenanthrene D-10 22.53 188 11422066 5.00 ug/L 0.00 20) Chrysene D-12 30.30 240 6020782 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.13 134 2094031 5.00 ug/L 0.00 Spiked Amount 5.000 Recovery = 100.00% 19) Triphenyl Phosphate surr 29.58 326 1617072 4.65 ug/L 0.00 Spiked Amount 5.000 Recovery = 93.00% 21) Perylene D-12 surr 34.31 264 3834598 4.82 ug/L 0.00 Spiked Amount 5.000 Recovery = 96.40%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 15.70 237 195348 0.84 ug/L 96 4) Hexachlorobenzene 21.39 284 534292 0.99 ug/L 98 5) EPTC 16.17 128 789268 1.01 ug/L 95 6) 2,6-Dinitrotoluene 17.77 165 230425 0.86 ug/L 97 7) 2,4-Dinitotoluene 18.91 165 249950 0.80 ug/L 92 8) Molinate 19.08 126 1147760 1.04 ug/L 99 10) Simazine 21.91 201 284248 0.92 ug/L 100 11) Atrazine 22.04 200 443659 1.09 ug/L 99 12) Alachlor 23.91 160 377872 0.96 ug/L 81 13) Terbacil 22.83 161 238953 0.95 ug/L 96 14) Acetochlor 23.69 146 241224 0.84 ug/L 98 15) Metribuzin 23.73 198 359266 0.82 ug/L 94 16) Metolachlor 24.84 162 1069652 0.84 ug/L 96 17) Butachlor 26.66 160 305041 0.83 ug/L 81 18) 4,4'-DDE 27.29 246 435568 0.98 ug/L 95 22) Bis (2-Ethylhexyl) adipate 29.52 129 703007 1.02 ug/L 99 23) Bis (2-Ethylhexyl) phthala 30.96 149 1107355 0.93 ug/L 98 24) Benzo (a) pyrene 34.16 252 992193 0.84 ug/L 98

0S 1. 30%

(#) = qualifier out of range (m) = manual integration CAL5A.D 121401.M Tue Dec 18 11:12:37 2001 Page 1

NYC-WTC_000058117

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NYC-WTC_000058117Source: NYC Law Department, mirrored locally

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