NYC-WTC_000055143
Laboratory calibration standard analysis for sample AD27491 showing response values for various compounds.
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Calibration standard results, sample AD27776, Dec 2001
Machine-extracted title · confidence 90%Laboratory calibration standard analysis for sample AD27776 showing response values for various compounds.
NYC-WTC_000055174–000055177Folder label: “525 X 11/19/01 A 12/6/01”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\MSDCHEM\1\DATA\12 0601\CAL5.D Vial: 14 Acq On 7 Dec 2001 2:26 am Operator: McLean Sample 2.0 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 12 11:49:14 2001 Quant Results File: 120501.RES
Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) Acenaphthene-diO 18.32 164 7339125 5.00 ug/L 0.00 9) Phenanthrene D-10 22.65 188 11298829 5.00 ug/L 0.00 20) Chrysene D-12 30.43 240 7105729 5.00 ug/L 0.00
System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 1496657 3.84 ug/L 0.00 Spiked Amount 5.000 Recovery = 76.80% 19) Triphenyl Phosphate surr 29.70 326 1972041 5.03 ug/L 0.01 Spiked Amount 5.000 Recovery = 100.60% 21) Perylene D-12 surr 34.45 264 4641250 4.65 ug/L 0.00 Spiked Amount 5.000 Recovery = 93.00%
Target Compounds Qvalue 3) Hexachlorocyclopentadiene 15.81 237 501426 2.22 ug/L 96 4) Hexachlorobenzene 21.51 284 1180920 2.15 ug/L 98 5) EPTC 16.28 128 1705727 2.21 ug/L 97 6) 2,6-Dinitrotoluene 17.89 165 456864 1.80 ug/L 94 7) 2,4-Dinitotoluene 19.10 165 428361 1.53 ug/L 96 8) Molinate 19.20 126 2466013 2.28 ug/L 96 10) Simazine 22.03 201 595152 1.88 ug/L 99 11) Atrazine 22.15 200 1037346 2.24 ug/L 99 12) Alachlor 24.02 160 1037827 2.43 ug/L 99 13) Terbacil 22.95 161 901491 1.87 ug/L 95 14) Acetochlor 23.80 146 701321 2.41 ug/L 92 15) Metribuzin 23.84 198 1134706 2.30 ug/L 99 16) Metolachlor 24.94 162 3272410 2.57 ug/L 99 17) Butachlor 26.77 160 959067 2.05 ug/L 91 18) 4,4'-DDE 27.40 246 1067707 2.28 ug/L 99 22) Bis (2-Ethylhexyl) adipate 29.62 129 2533504 2.44 ug/L 99 23) Bis (2-Ethylhexyl) phthala 31.07 149 4195014 2.38 ug/L 100 24) Benzo (a) pyrene 34.30 252 2059611 1.56 ug/L 97
N-2.6 Aye /
(#) = qualifier out of range (m) = manual integration CAL5.D 120501.M Thu Jan 10 09:48:23 2002 Page 1
NYC-WTC_000055175
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