Calibration standard analysis results, sample AD27547, Nov-Dec 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\120501\1116MDL.D Vial: 6 Acq On 5 Dec 2001 7:09 pm Operator:: McLean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO P Quant Time: Dec 11 09:27:34 2001 Quant Results File: 120501.RES Quant Method : C:\MSDCHEM\1\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501 Internal Standards R.T. Qlon Response Cone Units Dev (Min)

1) Acenaphthene-dlO 1.8,31 164 5215525 5.00 ug/L 0.00 9) Phenanthrene D-10 22.64 188 7782283 5.00 ug/L 0.00 2 0) Chrysene D-12 30.42 240 5455098 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 999658 3.61 ug/L 0.00 Spiked Amount 5.000 Recovery = 72.20% 19) Triphenyl Phosphate surr 29.69 326 1570140 5.82 ug/L 0.00 Spiked Amount 5.000 Recovery = 116.40% 21) Perylene D-12 surr 34.44 264 3606441 4.71 ug/L 0.00 Spiked Amount 5.000 Recovery = 94.20%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 15.81 237 1.6713 0.10 ug/L 86 4) Hexachlorobenzene 21.50 284 69665 0.18 ug/L 95 5) EPTC 16.2 8 128 434892 0.79 ug/L 97 6) 2,6-Dinitrotoluene 17.88 165 143177m 0.93 ug/L 7) 2,4-Dinitotoluene 19.05 165 111113m 0.75 ug/L 8) Molinate 19.19 126 738283 0.96 ug/L 99 10) Simazine 22.03 201 25514 0.12 ug/L 94 11) Atrazine 22.15 200 57630 0.18 ug/L 82 12) Alachlor 24.01 160 65087 0.22 ug/L 92 13) Terbacil 22.95 161 575243 1.73 ug/L 95 14) Acetochlor 23.80 ■146 415886 2.07 ug/L 93 15) Metribuzin 23.83 198 23495 0.07 ug/L 78 16) Metolachlor 24.94 162 158494 0.18 ug/L 95 17) Butachlor 26.76 160 74075 0.23 ug/L # 45 18) 4,4‘-DDE 27.40 246 229726 0.71 ug/L 94

(0.50 ug/LL# 22) Bis (2-Ethylhexyl) adipate 29.62 129 93187 0.22 66 23) Bis (2-Ethylhexyl) phthala 31.07 149 459157 97 24) Benzo (a) pyrene 34.29 252 60257 0.25 ug/L 94

(#) = qualifier out of range (m) = manual integration 1116MDL.D 120501. M Tue Dec 11 09:29:20 2001 Page 1

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