Laboratory report listing analytical results for pesticides and organic compounds in calibration standard AD27547.
NYC-WTC_000057727–000057729Folder label: “525 11/15/01 12/6 - 12/7 12/4 - 12/5 TWO INSTR.”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) Data File : C: \MSDCHEM\1\DATA\120501\CAL6 .D Vial: 4 Acq On : 5 Dec 2001 5:38 pm Operator: McLean Sample : 5.0 co ■ Inst : Instrumen Mise Multiply: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 11 09:18:20 2001 Quant Results File: 120501.RES
Quant Method : C:\MSDCHEM\1\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) Acenaphthene-diO 18.31 164 6382601 5.00 ug/L 0.00 9) Phenanthrene D-10 22.64 188 8945263 5.00 ug/L 0.00 20) Chrysene D-12 30.42 240 4551950 5.00 ug/L 0.00
System Monitoring Compounds 2) 1,3 -Dimethyl-2 -nitrobenzen 13.23 134 1257886 3.71 ug/L 0.00 Spiked Amount 5.000 Recovery = 74.20% 19) Triphenyl Phosphate surr 29.69 326 1675568 5.40 ug/L 0.00 Spiked Amount 5.000 Recovery = 108.00% 21) Perylene D-12 surr 34.44 264 4818293 7.54 ug/L 0.00 Spiked Amount 5.000 Recovery = 150.80%
Target Compounds Qvalue 3) Hexachlorocyclopentadiene 15.81 237 1305324 6.63 ug/L 97 4) Hexachlorobenzene 21.51 284 2370592 4.96 ug/L 97 5) EPTC 16.28 128 3570278 5.32 ug/L 99 6) 2,6-Dinitrotoluene 17.88 165 1244123 4.98 ug/L 97 7) 2,4-Dinitotoluene 19.03 165 1234918 4.20 ug/L 99 8) Molinate 19.20 126 5155440 5.47 ug/L 91 10) Simazine 22.04 201 1471307 5.87 ug/L 98 11) Atrazine 22.16 200 2283166 6.23 ug/L 97 12) Alachlor 24.02 160 2168655 6.41 ug/L 93 13) Terbacil 22.98 161 2163059 5.66 ug/L 100 14) Acetochlor 23.80 146 1496600 6.48 ug/L 99 15) Metribuzin 23.84 198 2666272 o i : ag/n ' 95 16) Metolachlor 24.94 162 6784795 ’ 3 uy/T 99 17) Butachlor 26.77 160 1961924 3.29 ug/L 86 18) 4,4'-DDE 27.40 246 2213634 5.98 ug/L 97 22) Bis (2-Ethylhexyl) adipate 29.62 129 4532620m 6.62 ug/L 23) Bls (2-Ethylhexyl) phthala 31.07 149 8086961m t ‘ i us/ L 24) Benzo (a) pyrene 34.29 252 5286074m 5.66 ug/L
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(#) = qualifier out of range (m) = manual integration CAL6.D 120501.M Tue Dec 11 14:57:50 2001 Page 1
NYC-WTC_000057728
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NYC-WTC_000055108
Calibration standard reference results for pesticide and organic compound analysis of sample AD27547, with measured values for 13 analytes including hexachlorobenzene (4.96 ug), si
1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000057734
Laboratory report listing analytical results for pesticides and organic compounds in recovery standard AD27547.
1 shared topics · Same agency, volume and box · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055828
Quality control report for calibration standards (AD28322) verifying instrument accuracy on December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055375
Quality control lab blank results for Method 525.2 showing detection limits for various pesticides and contaminants.
1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055804
Quality control report for calibration standards (AD28847) verifying instrument accuracy on December 20, 2001.
1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055825
Laboratory report for sample AD28322 showing non-detects for pesticides and contaminants analyzed on December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058063
Laboratory blank analysis results for sample AD28316 showing pesticide compound levels below detection limits on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055380
Calibration standard results for Method 525.2 listing concentrations and detection limits for target compounds.
1 shared topics · Same agency, volume and box · similarity 0.983
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000057057
Laboratory analysis of reference standard for sample AD27232 using EPA Method 525.2, dated Dec 13, 2001, showing detected levels of pesticides and organic compounds.
1 shared topics · Same agency, volume and box · similarity 0.983
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055433
Laboratory results for sample AD28045 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.983
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058107
Laboratory blank analysis results for sample AD28048 showing pesticide compound levels below detection limits on December 18, 2001.
1 shared topics · Same agency, volume and box · similarity 0.983
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055415
Laboratory results for sample AD27985 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.983
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NYC-WTC_000057711
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NYC-WTC_000057715
Log sheet recording laboratory extraction parameters for sample AD27547 processed between November and December 2001.
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NYC-WTC_000057724
Laboratory report listing analytical results for pesticides and organic compounds in calibration standard AD27547.
Filed in the same folder