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Pesticide control verification analysis, sample AD27546, Dec 2001

Machine-extracted title · confidence 95%

Lab quality control analysis verifying accuracy of pesticide detection methods for sample AD27546.

NYC-WTC_000057173–000057179

Folder label: “508 X 11/15/01 A 12/12 - 12/13/01

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\l\DATA\508\011212B\2PESTC2.D\ECDlA.CH Vial: 40 Signal #2 : C:\MSDCHEM\l\DATA\508\011212B\2PESTC2.D\ECD2B.CH Acq On : 13 Dec 2001 8:38 pm Operator: Nefliu Sample : pest ccv Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 26 14:27:24 2001 Quant Results File: 011212P.RES Quant Method : C:\MSDCHEM\1\METHODS\011212P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Wed Dec 26 14:11:58 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal 1 Phase Signal 2 Phase: Signal 1 Info Signal 2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.34 14.97 708.0E6 564.6E6 0.196 0.210 Spiked Amount 0.200 Recovery = 98.00% 105.00% Target Compounds 1) Propachlor 9.04 8.49 90103572 71576221 0.182 0.199 2) g-BHC 9.82 10.17 2164.7E6 1781.OE6 0.274 92. 0.310 3) Heptachlor 10.98 11.22 718.8E6 508.9E6 0.098/02/ 0.117 4) Aldrin 11.69 11.97 946.5E6 768.5E6 0.117^/- 0.126 5) Heptachlor Epoxi 13.13 13.33 1632.1E6 1322.4E6 0.2339 / 0.250 6) 4,4-DDE 13.96 14.54 2605.6E6 2153.5E6 0.387 97 0.415 7) Dieldrin 14.54 14.80 580.2E6 461.2E6 0.080 100/ 0.087 8) Endrin 15.04 15.46 1078.7E6 883.3E6 0.204 (6x, 0.225 9) Methoxychlor 16.99 18.01 992.6E6 628.6E6 0.417 (pl/* 0.482

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 2PESTC2.D 011212P.M Wed Dec 26 14:27:41 2001 Page 1

NYC-WTC_000057174

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NYC-WTC_000057174Source: NYC Law Department, mirrored locally

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