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← Document results/DEP Box 30/508 X 11/21/01 A 12/20 - 12/21/01
Document / 7 pages

Pesticide analysis results for sample AD27985, Nov-Dec 2001

Machine-extracted title · confidence 90%

Detailed laboratory report of pesticide and PCB analysis for sample AD27985, including surrogate recovery data.

NYC-WTC_000056433–000056439

Folder label: “508 X 11/21/01 A 12/20 - 12/21/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\l\DATA\508\011220B\2PESTC2.D\ECDlA.CH Vial: 33 Signal #2 : C:\MSDCHEM\1\DATA\ 508\011220B\2PESTC2.D\ECD2B.CH Acq On : 21 Dec 2001 3:49 am Operator: Nefliu Sample : pest ccv Inst : Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Jan 08 09:42:46 2002 Quant Results File: 011220P.RES

Quant Method : C:\MSDCHEM\1\METHODS\011220P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Fri Dec 21 08:18:43 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. : Signal #1 Phase : Signal #2 Phase: Signal #1 Info : Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/l ug/l

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.35 14.98 719.8E6 565.2E6 0.194m 0.202 Spiked Amount 0.200 Recovery = 97.00% 101.00%

Target Compounds 1) Propachlor 9.06 8.50 96300327 70994523 0.195 08 0.193 2) g-BHC 9.83 10.18 2290.3E6 1750.3E6 0.279 10 0.291 3) Heptachlor 11.00 11.23 716.6E6 452.8E6 0.096 (03 0.102 4) Aldrin 11.70 11.98 979.6E6 756.5E6 0.1190 0.120 5) Heptachlor Epoxi 13.14 13.34 1699.OE6 1296.6E6 0.23608 0.239 6) 4,4-DDE 13.97 14.55 2673.2E6 2088.6E6 0.394 9° 0.399 7) Dieldrin 14.55 14.81 607.6E6 461.2E6 0.077 1 0.080 8) Endrin 15.05 15.47 1149.1E6 862.8E6 0.203 167— 0.211 9) Methoxychlor 17.00 18.02 935.4E6 543.5E6 0.398 00 0.418

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 2PESTC2.D 011220P.M Tue Jan 08 09:43:26 2002 Page 1

NYC-WTC_000056434

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NYC-WTC_000056434Source: NYC Law Department, mirrored locally

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