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Pesticide analysis results below detection limits for sample AD28317

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Laboratory report indicating pesticide concentrations were below method detection limits for sample AD28317 collected in late 2001.

NYC-WTC_000056808–000056811

Folder label: “508 X 11/26/01 A 12/21 - 12/22/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\l\DATA\508\011221B\1126REFP.D\ECDlA.CH Vial: 31 Signal #2 : C:\MSDCHEM\l\DATA\508\011221B\1126REFP.D\ECD2B.CH Acq On : 22 Dec 2001 2:45 am Operator: Nefliu Sample : 11/26 ref pest Inst : Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Jan 09 10:19:52 2002 Quant Results File: 011220P.RES

Quant Method : C:\MSDCHEM\1\METHODS\011220P.M (Cherns tat ion Integrator) Title : 508 Chlorinated Pesticides Last Update : Fri Dec 21 08:18:43 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/l ug/l

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.35 14.98 656.3E6 526.3E6 0.177m 0.188 Spiked Amount 0.200 Recovery = 88.50% 94.00%

Target Compounds 1) Propachlor 9.06 8.50 151.5E6 120.5E6 0.307m 0.328 2) g-BHC 9.83 10.19 2294.7E6 1804.1E6 0.279m 0.300 3) Heptachlor 11.00 11.24 1316.2E6 889.3E6 0.177m 0.200 4) Aldrin 11.71 11.98 612.9E6 485.4E6 0.074m 0.077 5) Heptachlor Epoxi 13.14 13.34 1980.6E6 1604.7E6 0.275m 0.296 6) 4,4-DDE 13.97 14.55 5005.8E6 4008.8E6 0.739m 0.766 7) Dieldrin 14.56 14.81 1066.5E6 867.8E6 0.135m 0.151 8) Endrin 15.06 15.47 1132.4E6 893.9E6 0.200m 0.219 9) Methoxychlor 17.00 18.02 970.OE6 620.3E6 0.412m 0.477

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 1126REFP.D 011220P.M Wed Jan 09 10:20:43 2002 Page 1

NYC-WTC_000056810

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NYC-WTC_000056810Source: NYC Law Department, mirrored locally

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