Duplicate spiked sample analysis results, 525 X, Nov-Dec 2001

yudtLtdLLOL KEPOLL (NOC Kevlewed) Z 2 K - O Data File : C:\MSDCHEM\1\DATA\121201\27638.D Vial: 15 O

2 Acq On Sample : 12 Dec 2001 10:21 pm : sample Operator: Inst : McLean Instrumen co — o Mise : Multipir: 1.00 “0 1 C o MS Integration Params: BENZO.P O o o o Quant Time: Dec 12 22:58 2001 Quant Results File: 120501.RES o CH “O CH o O. Method : C:\MSDCHEM\l\5973N\121401.M (RTE Integrator) — CD Title : Quantitation For Method 525.2 0 O Last Update : Mon Dec 17 11:15:46 2001 o Q Response via : Initial Calibration C Abundance TIC: 27638.D 3 CD

7000000

6500000

6000000

5500000

5000000

4500000

4000000 8 Q

3 8 3500000 S co i I 3000000 i o § § o 2500000 3o s § s 2000000 CO I CM § 0 E § So 3

1500000 5 8 { g s CM

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% s s$ s 5 J 1 1000000 £ I i I g 1 5 8 § 4 4£ £ s <0

500000 s N s o Z I 5 8 2 5

O' L N ‘ I‘‘‘‘I+‘‘‘.‘‘1*I*1*‘I‘‘‘I‘‘‘*I‘‘‘I‘‘‘I‘‘‘I‘*II‘‘‘‘I‘‘‘I‘TItIII‘IIIIIIIIIII‘ 1 "I । । । i | । । । । p । । i | 1 I I । | । i i i | । Time—> 12.00 13.00 14.00 15.00 16.00 17.00 18.00 19.00 20.00 21.00 22.00 23.00 24.00 25.00 26.00 27.00 28.00 29.00 30.00 31.00 32.00 33.00 34.00 35.00 36.00

27638.D 121401.M Mon Dec 17 13:22:35 2001 Page 2