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ICPMS daily performance check report, May 22, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 22, 2002.

NYC-WTC_000054157–000054373

Folder label: “ICPMS 5/22/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE11304 Sample Date/Time: Wednesday, May 22, 2002 10:08:06 Sample Type: Spike -1 Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE11304.286 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 17254.536 2.075 0.371 51.50734 1.38 ug/L Li 6 46545.994 1.043 46545.994 ug/L Sc-1 45 363846.985 2.313 363846.985 ug/L Cr 52 375156.764 1.701 1.015 49.06435 1.19 ug/L Cr 53 44836.464 2.753 0.122 49.08685 0.44 ug/L Mn 55 891117.097 3.185 2.446 71.35674 1.08 ug/L Co 59 451088.876 2.176 1.239 49.92506 0.75 ug/L Ni 60 94180.336 1.444 0.259 49.97747 0.93 ug/L Cu 63 213396.518 1.122 0.586 51.57012 1.26 ug/L Cu 65 104182.784 2.121 0.286 51.15645 0.39 ug/L Zn 66 74233.288 1.267 0.870 52.48597 2.59 ug/L Zn 67 13042.151 3.039 0.153 51.78035 0.77 ug/L Zn 68 55680.579 1.523 0.652 52.62436 2.90 ug/L > Ge 72 84728.894 3.779 84728.894 ug/L As 75 100591.111 1.277 1.051 52.13533 3.77 ug/L Se 77 9988.885 1.337 0.101 54.49077 3.07 ug/L Se 82 10159.470 1.641 0.120 54.99952 4.52 ug/L As-1 75 85248.720 1.119 85091.717 49.63460 1.12 ug/L Kr 83 4314.067 1.403 -328.166 ug/L Ag 107 403685.021 0.972 0.344 42.89523 1.59 ug/L Cd 111 120765.437 1.077 0.103 50.13247 0.08 ug/L Cd 114 287067.221 1.645 0.245 50.44193 1.48 ug/L In 115 1171474.676 0.997 1171474.676 ug/L Sb 121 413904.160 2.294 0.353 52.18955 1.34 ug/L Sb 123 316830.304 0.693 0.270 51.86095 0.49 ug/L Ba 135 152962.717 0.908 0.085 65.54148 1.41 ug/L Ba 137 266658.000 1.228 0.149 65.36422 0.36 ug/L Ho 165 1816130.527 0.373 0.012 ug/L Tb 159 1791481.283 1.365 1791481.283 ug/L Hg 201 5829.594 1.612 0.003 4.37990 1.95 ug/L Hg 202 13131.611 1.979 0.007 4.37204 1.77 ug/L TI 205 1357920.810 0.858 0.758 48.47844 0.58 ug/L Pb 208 1847480.832 0.985 1.030 48.59110 0.38 ug/L

Sample ID: AE11304 Report Date/Time: Wednesday, May 22, 2002 10:10:40 Page 1

NYC-WTC_000054191

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NYC-WTC_000054191Source: NYC Law Department, mirrored locally

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