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ICPMS daily performance check report, May 16, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 16, 2002.

NYC-WTC_000053706–000053937

Folder label: “ICPMS 5/16/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10160 Sample Date/Time: Thursday, May 16, 2002 11:10:31 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: C:\WINNT\Profiles\lrd1\Elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE101 60.147 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 8.000 25,000 0.000- 0.00249 208.61 ug/L Li 6 53732.869 0.587 53732.869 ug/L > Sc-1 45 409970.396 0.833 409970.396 ug/L Cr 52 8054.314 1.124 0.005 0.22274 7.14 ug/L Cr 53 1612.159 4.209 0.002 0.84337 7 86 ug/L Mn 55 301380.450 1.731 0.732 20.58649 2.58 ug/L Co 59 397.013 4.304 0,000 0.01891 8.37 ug/L Ni 60 751.039 2.441 0.002 0.33539 3.40 ug/L Cu 63 7435.114 0.543 0.018 1.53787 0.78 ug/L Cu 65 3607.752 1.151 0.009 1.51866 1.86 ug/L Zn 66 4525.505 2.273 0.040 2.33836 1.12 ug/L Zn 67 899.387 1.481 0.008 2.63285 2.72 ug/L Zn 68 3810.503 0.859 0.034 2.69177 1.15 ug/L > Ge 72 93766.793 1.796 93766.793 ug/L As 75 5429.175 2.740 0.008 0.38410 7.32 ug/L Se 77 739.969 1.569 0.001 0.47211 8.61 ug/L Se 82 -33.818 46.402 -0.000 -0.07308 102.17 ug/L As-1 75 799.710 3.819 601.706 0.29347 5.08 ug/L Kr 83 1933.558 1.157 -95.355 ug/L Ag 107 203.004 22.124 -0.000 -0.05339 7.73 ug/L Cd 111 111.002 19.552 0.000 0.01155 67.46 ug/L Cd 114 264.323 13.042 0.000 0.01666 31.09 ug/L > In 115 1281755.803 0.902 1281755.803 ug/L Sb 121 474.017 4.009 0.000 0.04893 4.47 ug/L Sb 123 347.617 4.395 0.000 0.04592 5.52 ug/L Ba 135 45292.680 1.329 0.024 17.10704 1.63 ug/L Ba 137 78125.379 0.587 0.042 16.91265 0.87 ug/L Ho 165 1898560.730 0.663 -0.003 ug/L > Tb 159 1873816.261 0.691 1873816.261 ug/L Hg 201 31.334 17.577 -0.000 -0.00684 57.58 ug/L Hg 202 81.668 1.870 0.000 0.00042 144.03 ug/L TI 205 572.690 5.611 -0.000 -0.00379 28.31 ug/L Pb 208 4509.146 1.063 0.001 0.06278 2.47 ug/L

Sample ID: AE10160 Report Date/Time: Thursday, May 16,2002 11:12:28 Page 1

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