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ICPMS daily performance check report, May 16, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 16, 2002.

NYC-WTC_000053706–000053937

Folder label: “ICPMS 5/16/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: Standard 1 Sample Date/Time: Thursday, May 16,2002 09:23:36 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\Standard 1.127 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 12610.200 1.399 0.218 - 30.80474 0.39 ug/L Li 6 57945.368 1.786 57945.368 ug/L > Se-1 45 468717.146 1.883 468717.146 ug/L Cr 52 300225.330 1.219 0.626 29.72144 0.72 ug/L Cr 53 36257.884 2.389 0.076 29.56284 1.70 ug/L Mn 55 503566.033 1.462 1.071 30.12943 0.43 ug/L Co 59 362627.003 2.329 0.773 30.34389 2.92 ug/L Ni 60 75007.432 3.029 0.160 30.15523 1.22 ug/L Cu 63 162901.302 2.192 0.347 30.50014 0.88 ug/L Cu 65 79871.542 1.832 0.170 30.68654 1.73 ug/L Zn 66 53824.091 1.407 0.510 30.41361 0.78 ug/L Zn 67 9459.349 2.860 0.089 29.97130 2.63 ug/L Zn 68 39978.790 1.379 0.378 29.99972 0.59 ug/L > Ge 72 103967.860 0.837 103967.860 ug/L As 75 68597.826 2.514 0.610 29.59691 2.21 ug/L Se 77 6630.176 1.740 0.057 29.71122 1.29 ug/L Se 82 6908.000 1.971 0.067 29.62973 1.35 ug/L As-1 75 61205.026 2.337 61007.022 31.36597 2.34 ug/L Kr 83 2021.578 2.249 -7.335 ug/L Ag 107 339013.519 1.876 0.238 29.80557 2.65 ug/L Cd 111 88625.898 1.976 0.062 29.87055 1.46 ug/L Cd 114 207961.805 2.553 0.146 29.82460 1.20 ug/L > In 115 1419331.178 1.995 1419331.178 ug/L Sb 121 280440.232 0.995 0.198 30.34310 1.71 ug/L Sb 123 215591.977 1.298 0.152 30.50392 1.00 ug/L Ba 135 83223.413 1.403 0.043 31.40436 1.08 ug/L Ba 137 145528.660 2.023 0.075 31.51662 1.53 ug/L Ho 165 1994347.907 1.088 0.008 ug/L > Tb 159 1947648.690 1.079 1947648.690 ug/L Hg 201 3227.272 2.214 0.002 2.27152 1.67 ug/L Hg 202 7132.202 1.816 0.004 2.22979 0.84 ug/L TI 205 956009.299 0.864 0.491 31.90284 0.93 ug/L Pb 208 1304557.068 0.984 0.669 31.45537 0.85 ug/L

QC Calculated Values

Sample ID: Standard 1 Report Date/Time: Thursday, May 16, 2002 09:25:33 Page 1

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