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ICPMS daily performance check report, May 16, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 16, 2002.

NYC-WTC_000053706–000053937

Folder label: “ICPMS 5/16/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10020 Sample Date/Time: Thursday, May 16, 2002 10:51:47 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: C:\WINNT\Profiles\lrd1\Elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE1 0020.141 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 12.333 18.725 0.000- 0.01511 40.32 ug/L Li 6 51851.306 0.750 51851.306 ug/L Sc-1 45 405138.731 0.751 405138.731 ug/L Cr 52 9467.358 3.218 0.008 0.39785 10.58 ug/L Cr 53 1470.800 2.756 0.002 0.72407 6.96 ug/L Mn 55 225359.703 0.566 0.553 15.55119 1.32 ug/L Co 59 366.678 5.730 0.000 0.01645 12.86 ug/L Ni 60 770.707 3.872 0.002 0.34865 3.38 ug/L Cu 63 6249.879 3.911 0.015 1.30257 4.16 ug/L Cu 65 3042.540 1.120 0.007 1.28991 0.60 ug/L Zn 66 2743.775 1.376 0.021 1.23473 4.65 ug/L Zn 67 605.026 9.060 0.005 1.59914 12.97 ug/L Zn 68 2432.350 4.713 0.020 1.54066 3.74 ug/L > Ge 72 93682.305 2.154 93682.305 ug/L As 75 5503.982 3.617 0.009 0.42494 10.94 ug/L Se 77 748.859 3.348 0.001 0.52401 13.77 ug/L Se 82 -40.054 142.380 -0.000 -0.09893 269.13 ug/L As-1 75 805.710 2.229 607.706 0.29640 2.95 ug/L Kr 83 1960.565 4.324 -68.349 ug/L Ag 107 444.349 23.320 -0.000 -0.03011 33.59 ug/L Cd 111 123.002 18.414 0.000 0.01647 52.79 ug/L Cd 114 279.272 16.324 0.000 0.01943 37.39 ug/L > In 115 1271331.474 1.065 1271331.474 ug/L Sb 121 613.694 0.898 0.000 0.06563 0.25 ug/L Sb 123 473.921 4.270 0.000 0.06549 3.72 ug/L Ba 135 44417.020 0.249 0.024 16.78848 1.59 ug/L Ba 137 77139.330 0.258 0.041 16.71169 1.60 ug/L Ho 165 1893362.496 1.898 -0.005 ug/L > Tb 159 1872608.689 1.334 1872608.689 ug/L Hg 201 50.667 11.565 0.000 0.00656 67.31 ug/L Hg 202 124.002 5.645 0.000 0.01330 16.92 ug/L n 205 626.361 6.137 -0.000 -0.00202 51.72 ug/L Pb 208 4712.861 2.325 0.001 0.06778 2.34 ug/L

Sample ID: AE10020 Report Date/Time: Thursday, May 16, 2002 10:53:44 Page 1

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