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ICPMS daily performance check report, May 16, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 16, 2002.

NYC-WTC_000053706–000053937

Folder label: “ICPMS 5/16/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09683 Sample Date/Time: Thursday, May 16, 2002 10:23:44 Sample Type: Sample Sample Description: Zn Number of Replicates: 3 Method File: C:\WINNT\Profiles\lrd1\Elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE09683.138 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 4.333 74.182 -0.000- -0.00752 110.97 ug/L Li 6 55524.988 2.129 55524.988 ug/L > Se-1 45 443530.765 1.802 443530.765 ug/L Cr 52 14029.626 1.706 0.017 0.78647 4.09 ug/L Cr 53 2622.071 1.500 0.004 1.62740 4.71 ug/L Mn 55 740561.897 1.653 1.666 46.88476 1.25 ug/L Co 59 827.713 1.927 0.001 0.05394 3.57 ug/L Ni 60 3317.305 1.326 0.007 1.40759 1.85 ug/L Cu 63 31532.589 2.069 0.071 6.14058 3.76 ug/L Cu 65 14981.486 1.725 0.034 -__ _ 3.51 ug/L Zn 66 2852.810 2.835 0.021 1.19750 3.20 ug/L Zn 67 792.709 3.242 0.006 2.09604 5.50 ug/L Zn 68 2998.858 1.726 0.024 1.8678 0.70 ug/L > Ge 72 99526.882 1.181 99526.882 ug/L As 75 5586.794 4.009 0.006 0.29862 28.27 ug/L Se 77 846.929 4.411 0.002 0.78990 19.20 ug/L Se 82 -11.694 716.741 0.000 0.03102 1178.81 ug/L As-1 75 1299.106 2.737 1101.102 0.53704 3.23 ug/L Kr 83 1958.231 3.393 -70.683 ug/L Ag 107 1520.142 4.546 0.001 0.06491 8.21 ug/L Cd 111 102.668 13.152 0,000 0.00668 64.25 ug/L Cd 114 221.369 6.844 0,000 0.00819 22.66 ug/L > In 115 1343027.950 1.450 1343027.950 ug/L Sb 121 856.382 3.010 0.001 0.08858 4.17 ug/L Sb 123 672.057 6.503 0.000 0.09018 8.34 ug/L Ba 135 78695.626 1.131 0.039 27.74875 0.39 ug/L Ba 137 137083.235 0.938 0.068 27.70572 1.20 ug/L Ho 165 2061617.734 0.987 0.011 ug/L > Tb 159 2007665.873 0.768 2007665.673 ug/L Hg 201 110.002 16.160 0.000 0.04241 26.04 ug/L Hg 202 215.671 7.539 0.000 0.03671 12.01 ug/L n 205 499.685 10.050 -0.000 -0.00730 19.63 ug/L Pb 208 37775.284 16.426 0.018 0.80990 18.24 ug/L

Sample ID: AE09683 Report Date/Time: Thursday, May 16, 2002 10:26:36 Page 1

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