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ICPMS daily performance check report, May 16, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 16, 2002.

NYC-WTC_000053706–000053937

Folder label: “ICPMS 5/16/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: ICV STD2 60+5 PPB Sample Date/Time: Thursday, May 16,2002 09:47:17 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\ICV STD2 60+5 PPB.131 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 23908.978 1.784 0.433 ' 61.44191 0.84ug/L Li 6 55208.693 0.959 55208.693 ug/L > Sc-1 45 448972.993 1.868 448972.993 ug/L Cr 52 575421.861 1.305 1.267 59.56969 1.66 ug/L Cr 53 67631.009 1.426 0.149 58.89106 0.92 ug/L Mn 55 941716.977 3.748 2.094 58.91723 3.05 ug/L Co 59 682742.762 1.646 1.520 59.27971 1.56 ug/L Ni 60 143161.513 2.117 0.319 60.52212 1.88 ug/L Cu 63 315237.413 3.036 0.702 60.95835 3.09 ug/L Cu 65 153234.858 0.410 0.341 60.44961 2.29 ug/L Zn 66 104033.935 0.691 1.022 59.49884 1.02 ug/L Zn 67 18032.383 1.600 0.177 58.41313 1.53 ug/L Zn 68 76972.946 0.976 0.756 59.24760 0.43 ug/L > Ge 72 100983.135 0.864 100983.135 ug/L As 75 128452.315 0.931 1.222 59.00482 0.78 ug/L Se 77 12322.309 0.715 0.115 59.38088 1.57 ug/L Se 82 13804.589 0.841 0.137 59.74356 1.66 ug/L As-1 75 118412.500 1.606 118214.496 57.65714 1.61 ug/L Kr 83 1957.230 1.155 -71.683 ug/L Ag 107 691379.893 0.450 0.499 60.59421 0.64 ug/L Cd 111 172990.562 1.025 0.125 59.84100 0.72 ug/L Cd 114 399881.872 1.042 0.289 59.12821 0.80 ug/L > In 115 1384766.159 0.483 1384766.159 ug/L Sb 121 556584.915 0.563 0.402 59.45529 0.08 ug/L Sb 123 429893.328 0.768 0.310 59.85998 0.34 ug/L Ba 135 163098.085 0.965 0.083 58.52192 1.65 ug/L Ba 137 282168.829 2.380 0.143 58.02064 1.98 ug/L Ho 165 2009037.422 1.303 0.002 ug/L > Tb 159 1973664.444 0.785 1973664.444 ug/L Hg 201 7318.352 1.867 0.004 4.77480 2.43 ug/L Hg 202 16765.280 1.062 0.008 4.80564 1.83 ug/L TI 205 1834225.355 1.473 0.929 57.29891 2.17 ug/L Pb 208 2520001.272 1.005 1.276 58.03394 1.57 ug/L

Sample ID: ICV STD2 60+5 PPB Report Date/Time: Thursday, May 16, 2002 09:50:06 Page 1

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