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ICPMS daily performance check report, May 16, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 16, 2002.

NYC-WTC_000053706–000053937

Folder label: “ICPMS 5/16/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10242 Sample Date/Time: Thursday, May 16, 2002 12:20:59 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: C:\WINNT\Profiles\lrd1\Elandata\MethodVNEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE10242.165 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 7.000 37.796 0.000 0.00066 1119.78 ug/L Li 6 51573.398 0.900 51573.398 ug/L > Se-1 45 411535.899 1.406 411535.899 ug/L Cr 52 12244.029 0.589 0.015 0.69808 3.78 ug/L Cr 53 2519.041 1.871 0.004 1.71002 4.67 ug/L Mn 55 728830.998 2.098 1.767 49.73290 1.67 ug/L Co 59 824.379 1.656 0.002 0.05926 1.10 ug/L Ni 60 14758.786 1.085 0.036 6.79560 0.68 ug/L Cu 63 17834.662 2.488 0.043 3.72669 1.77 ug/L Cu 65 8364.932 2.435 0.020 3.56075 1.95 ug/L Zn 66 2019.578 3.837 0.014 0.82186 7.18 ug/L Zn 67 639.029 1.364 0.005 1.78538 2.67 ug/L Zn 68 2297.647 1.590 0.019 1.48621 1.76 ug/L > Ge 72 90955.332 0.755 90955.332 ug/L As 75 5395.229 2.071 0.009 0.45308 16.40 ug/L Se 77 815.932 1.566 0.002 1.02903 8.26 ug/L Se 82 -58.316 123.737 -0.000 -0.19398 177.61 ug/L As-1 75 1190.757 3.988 992.752 0.48420 4.78 ug/L Kr 83 1951.896 2.160 -77.018 ug/L Ag 107 91.335 2.279 -0.001 -0.06351 0.46 ug/L Cd 111 73.334 16.439 -0.000 -0.00111 407.82 ug/L Cd 114 162.668 13.955 0.000 0.00175 206.79 ug/L In 115 1219368.427 1.102 1219368.427 ug/L Sb 121 647.363 6.645 0.000 0.07273 6.17 ug/L Sb 123 489.625 7.362 0.000 0.07106 8.19 ug/L Ba 135 74903.746 0.929 0.041 29.21258 0.61 ug/L Ba 137 131273.973 2.286 0.072 29.34348 2.16 ug/L Ho 165 1833657.914 1.083 -0.006 ug/L > Tb 159 1815228.167 0.331 1815228.167 ug/L Hg 201 45.001 12.373 0.000 0.00359 111.84 ug/L Hg 202 91.335 8.071 0.000 0.00424 52.64 ug/L TI 205 353.010 8.447 -0.000 -0.01065 9.16 ug/L Pb 208 11951.857 1.006 0.006 0.25280 0.81 ug/L

Sample ID: AE10242 Report Date/Time: Thursday, May 16, 2002 12:22:56 Page 1

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