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ICPMS daily performance check report, May 15, 2002

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Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 15, 2002.

NYC-WTC_000053505–000053628

Folder label: “ICPMS 5/15/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: Standard 2 Sample Date/Time: Wednesday, May 15, 2002 09:44:52 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york city\Standard 2.060 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 26154.164 0.836 0.424 ' 60.07262 1.10 ug/L Li 6 61733.896 1.863 61733.896 ug/L Se-1 45 517082.536 0.798 517082.536 ug/L Cr 52 671422.018 0.735 1.282 60.06260 1.38 ug/L Cr 53 80907.642 1.664 0.156 60.42475 1.68 ug/L Mn 55 1127951.626 2.009 2.179 60.39372 2.33 ug/L Co 59 802508.781 0.684 1.552 60.28627 1.36 ug/L Ni 60 166690.902 1.570 0.322 60.16412 2.04 ug/L Cu 63 365173.992 0.518 0.706 60.13631 0.68 ug/L Cu 65 177297.271 2.422 0.343 60.11146 1.89 ug/L Zn 66 116893.938 0.975 1.001 59.92653 0.31 ug/L Zn 67 20583.816 0.497 0.176 59.66743 1.52 ug/L Zn 68 88020.279 0.465 0.753 59.77946 0.69 ug/L > Ge 72 116005.335 1.110 116005.335 ug/L As 75 146832.609 0.551 1.218 59.94901 0.58 ug/L Se 77 13576.226 1.359 0.110 59.37694 0.29 ug/L Se 82 15510.846 0.737 0.134 59.76572 0.41 ug/L As-1 75 136045.099 0.555 135919.763 59.81864 0.56 ug/L Kr 83 2130.938 0.856 -70.684 ug/L Ag 107 767915.445 0.993 0.487 60.24152 1.33 ug/L Cd 111 195661.762 1.528 0.126 59.88127 1.54 ug/L Cd 114 453668.307 0.876 0.293 59.84702 1.31 ug/L In 115 1547742.735 2.149 1547742.735 ug/L Sb 121 587274.040 1.839 0.379 59.53552 0.89 ug/L Sb 123 452395.231 2.074 0.292 59.65582 0.61 ug/L Ba 135 182540.439 1.276 0.090 59.48850 1.22 ug/L Ba 137 320467.963 1.180 0.157 59.60952 0.93 ug/L Ho 165 2068711.839 0.784 0.001 ug/L Tb 159 2036596.775 0.480 2036596.775 ug/L Hg 201 7818.106 1.624 0.004 4.96238 1.89 ug/L Hg 202 17689.705 0.725 0.009 4.95201 0.84 ug/L TI 205 1915596.241 0.906 0.940 58.58050 1.39 ug/L Pb 208 2783652.730 0.280 1.365 59.54471 0.76 ug/L

QC Calculated Values

Sample ID: Standard 2 Report Date/Time: Wednesday, May 15, 2002 09:46:48 Page 1

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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