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ICPMS daily performance check report, May 15, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 15, 2002.

NYC-WTC_000053505–000053628

Folder label: “ICPMS 5/15/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10200 Sample Date/Time: Wednesday, May 15, 2002 11:16:02 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork city\AE1 0200.078 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 7.667 32.825 -0.000 -0.00856 76.11 ug/L Li 6 55471.993 2.003 55471.993 ug/L > Sc-1 45 452853.484 0.662 452853.484 ug/L Cr 52 8688.571 1.654 0.004 0.17439 7.43 ug/L Cr 53 2086.594 2.345 0.004 1.39222 2.20 ug/L Mn 55 320925.755 1.845 0.705 19.54171 2.42 ug/L Co 59 407.680 5.827 0.001 0.02481 9.17 ug/L Ni 60 1000.065 2.762 0.002 0.39481 3.55 ug/L Cu 63 227530.928 0.970 0.502 42.75057 1.58 ug/L Cu 65 112841.124 0.118 0.249 43.64631 0.56 ug/L Zn 66 11920.263 0.979 0.106 6.34405 2.68 ug/L Zn 67 1989.238 0.697 0.017 5.86854 2.37 ug/L Zn 68 9105.649 1.234 0.081 6.39121 1.68 ug/L Ge 72 105377.701 1.537 105377.701 ug/L As 75 5823.509 3.403 0.007 0.34119 17.76 ug/L Se 77 824.766 2.705 0.001 0.54422 9.73 ug/L Se 82 27.518 220.746 0.001 0.27378 94.53 ug/L As-1 75 1273.102 • 1.635 1151.100 0.50660 1.81 ug/L Kr 83 1934.892 1.672 -166.372 ug/L Ag 107 102.002 11.927 -0.000 -0.03297 2.95 ug/L Cd 111 96.335 14.321 0.000 0.00512 88.26 ug/L Cd 114 231.911 6.723 0.000 0.01026 19.77 ug/L > In 115 1434816.322 1.124 1434816.322 ug/L Sb 121 499.019 9.054 0.000 0.04957 10.47 ug/L Sb 123 405.323 5.572 0.000 0.05242 7.18 ug/L Ba 135 47690.917 1.025 0.024 15.96221 0.69 ug/L Ba 137 83198.178 1.324 0.042 15.89729 1.87 ug/L Ho 165 2031478.584 1.201 0.009 ug/L > Tb 159 1980624.463 0.620 1980624.463 ug/L Hg 201 50.667 10.870 -0.000 -0.01175 30.25 ug/L Hg 202 108.002 9.623 -0.000 -0.01188 26.98 ug/L TI 205 584.025 9.936 -0.000 -0.00424 40.91 ug/L Pb 208 11285.198 1.160 0.004 0.19473 1.11 ug/L

QC Calculated Values

Sample ID: AE10200 Report Date/Time: Wednesday, May 15, 2002 11:17:58 Page 1

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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