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ICPMS daily performance check report, May 15, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 15, 2002.

NYC-WTC_000053505–000053628

Folder label: “ICPMS 5/15/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10199 Sample Date/Time: Wednesday, May 15, 2002 11:12:45 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profilesMrd1\elandata\Dataset\newyork cit\AE1 0199.077 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean IMeas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 8.333 42.143 -0.000- -0.00668 136.49 ug/L Li 6 54963.207 0.788 54963.207 ug/L > Se-1 45 440721.834 0.290 440721.834 ug/L Cr 52 9858.108 1.387 0.007 0.32353 4.63 ug/L Cr 53 2149.276 2.016 0.004 1.49694 2.88 ug/L Mn 55 343268.240 1.076 0.775 21.48567 1.09 ug/L Co 59 533.688 5.471 0.001 0.03687 6.97 ug/L Ni 60 10969.396 3.549 0.025 4.62833 3.27 ug/L Cu 63 154072.138 2.756 70.349 29.72075 2.49 ug/L Cu 65 74753.354 3.074 / 0.169 29.68075 2.82 ug/L Zn 66 1 20023.232 =— 1.775 / 0.187 11.17686 0.99 ug/L Zn 67 3287.627 1.451 / 0.030 10.25659 2.79 ug/L Zn 68 15243.593 2.426 / 0.142 11.24956 3.57 ug/L > Ge 72 103286.621 2.049 103286.621 ug/L As 75 5971.559 1.907 0.010 0.46848 21.68 ug/L Se 77 839.384 2.658 0,001 0.70790 23.01 ug/L Se 82 -20.867 384,957 0.000 0.07276 476.15 ug/L As-1 75 1268.768 .105 1146.766 0.50469 1.22 ug/L Kr 83 2016.244 1.907 -85.020 ug/L Ag 107 157.336 3.199 -0.000 0.02793 2.30 ug/L Cd 111 106.002 5.253 0.000 0.00896 23.48 ug/L Cd 114 257.461 7.658 0.000 0.01455 16.08 ug/L > In 115 1409030.492 1.465 1409030.492 ug/L Sb 121 525.354 3.386 0.000 0.05348 2.96 ug/L Sb 123 413.451 2.622 0.000 0.05464 3.83 ug/L Ba 135 50386.42& 1.104 0.026 16.97393 0.99 ug/L Ba 137 88412.472 1.727 0.045 17.00187 1.61 ug/L Ho 165 2002540,681 0.448 0.001 ug/L > Tb 159 1968139.873 1.264 1968139.873 ug/L Hg 201 45.334 29.126 -0.000 -0.01510 56.; ug/L Hg 202 104.002 12.500 -0.000 -0.01283 32.41 ug/L TI 205 602.359 9.439 -0.000 -0.00355 45.12 ug/L Pb 208 6107.529 3.181 0.002 0.08156 3.22 ug/L

QC Calculated Values

Sample ID:AE10199 Report Date/Time: Wednesday, May 15, 2002 11:14:41 Page 1

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NYC-WTC_000053630 · Box DEP Box 29

Laboratory analysis results for a Westchester County Department of Labs and Research sample processed on May 15, 2002.

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